Synlett 2019; 30(08): 955-960
DOI: 10.1055/s-0037-1611758
letter
© Georg Thieme Verlag Stuttgart · New York

Visible-Light-Mediated Tandem Sulfonylation/Cyclization of Vinyl Azides with Sulfonyl Hydrazines for the Synthesis of 6-(Sulfonylmethyl)phenanthridines under Mild Conditions

Liu-Liang Mao*
a   Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao 334001, P. R. of China   eMail: maoll14@lzu.edu.cn   eMail: zhouanxi@hotmail.com
,
Li-Xia Quan
b   Shangrao Normal University, College of Chemistry and Environment Science, Shangrao 334001, P. R. of China
,
Xian-Hong Zhu
a   Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao 334001, P. R. of China   eMail: maoll14@lzu.edu.cn   eMail: zhouanxi@hotmail.com
,
Cong-Bin Ji
b   Shangrao Normal University, College of Chemistry and Environment Science, Shangrao 334001, P. R. of China
,
a   Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao 334001, P. R. of China   eMail: maoll14@lzu.edu.cn   eMail: zhouanxi@hotmail.com
,
Fayun Chen
b   Shangrao Normal University, College of Chemistry and Environment Science, Shangrao 334001, P. R. of China
,
Da-Gui Zheng
a   Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi Province, Shangrao Normal University, Shangrao 334001, P. R. of China   eMail: maoll14@lzu.edu.cn   eMail: zhouanxi@hotmail.com
› Institutsangaben
GJJ161059This work was supported by the Science and Technology Research Projects of the Education Department of Jiangxi Province, (Grant/Award Nos.: GJJ14716, GJJ151062, GJJ161059, GJJ161059)
Weitere Informationen

Publikationsverlauf

Received: 31. Januar 2019

Accepted after revision: 27. Februar 2019

Publikationsdatum:
10. April 2019 (online)


Abstract

A visible-light-mediated tandem sulfonylation/cyclization of vinyl azides with sulfonyl hydrazines was developed that provides an efficient and simple strategy for the synthesis of valuable 6-(sulfonylmethyl)phenanthridines with a broad substrate scope and satisfactory yields under mild conditions.

Supporting Information