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Synlett 1993; 1993(12): 933-934
DOI: 10.1055/s-1993-22658
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An Efficient Palladium-Catalyzed Synthesis of γ,δ-Alkenyl-1,1-Bisphosphonates

Richard Sulsky* , David R. Magnin
  • *Bristol-Myers Squibb Pharmaceutical Research Institute, P. 0. Box 4000, Princeton, NJ 08543, USA
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Publication Date:
19 March 2002 (online)

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The palladium-catalyzed coupling of allylic acetates with tetraethyl methylenebisphosphonate and O,N-bis(trimethylsilyl)acetamide generates mono-alkylated γ,δ-alkenyl-1,1-bisphosphonates in moderate to high yields.

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