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Synthesis 1995; 1995(10): 1243-1244
DOI: 10.1055/s-1995-4093
short paper
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Phosphorothioate Synthesis Based on the Redox Reaction of Phosphite with Tellurium(IV) Chloride

Yutaka Watanabe* , Shinji Inoue, Takashi Yamamoto, Shoichiro Ozaki
  • *Department of Applied Chemistry, Faculty of Engineering, Ehime University, Matsuyama 790-77, Japan, Fax +81(899)230672
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Publication Date:
31 December 2000 (online)

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Phosphoric thiol esters are conveniently prepared by the treatment of phosphorous triesters with thiols in the presence of tellurium(IV) chloride in a redox-type reaction.

redox reaction - phosphite - thiol - tellurium(IV) chloride - phosphorothioate