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Synlett 1995; 1995(8): 861-862
DOI: 10.1055/s-1995-5101
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Microwave-induced Rapid Synthesis of Bile acid Conjugates

B. Dayal* , K. R. Rapole, G. Salen, S. Shefer, G. S. Tint, S. R. Wilson
  • *Department of Medicine, University of Medicine and Dentistry of New Jersey, New Jersey Medical School, Newark, N.J. 07103; Veterans Administration Medical Center, East Orange, N.J. 07019
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Publication Date:
31 December 2000 (online)

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Efficient syntheses of a wide variety of glycine and taurine conjugated bile acids were achieved in absolute ethanol in a domestic microwave oven. The title compounds were characterized by proton nuclear magnetic resonance and electrospray ionization mass spectrometry.

Microwave oven - glycine and taurine conjugated bile acids - electrospray ionization mass spectrometry