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Synlett 2000; 2000(9): 1281-1282
DOI: 10.1055/s-2000-7138
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Ferric Chloride: a New and Very Efficient Catalyst for the Ferrier Glycosylation Reaction

Christophe Masson* , Javier Soto, Michel Bessodes
  • *Laboratoire de Vectorologie Moléculaire et Cellulaire UMR7001 ENSCP/CNRS/Aventis Pharma Gencell, 13 quai Jules Guesde, 94403 Vitry/Seine cedex France; Fax 33 (1) 55 71 81 32; E-mail: michel.bessodes@aventis.com
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Publication Date:
31 December 2000 (online)

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Reaction of tri-O-acetyl-d-glucal with different alcohols, in the presence of catalytic amounts of ferric chloride, led to the corresponding 2,3-unsaturated glycosides. The influence of solvent, temperature and amount of catalyst on the reaction was investigated.

glycosylations - catalysis - stereoselectivity - solvent effects - iron