PDF herunterladen
CC BY-NC-ND 4.0 · Eur J Dent 2010; 04(02): 183-191
DOI: 10.1055/s-0039-1697828
Original Article
European Journal of Dentistry

Effect of Energy Density on the Physical Properties of Resin-Based Restorative Materials when Polymerized with Quartz-Tungsten Halogen or LED-Light

Stefan Ruttermann
a   Heinrich-Heine-University, Medical Faculty, Centre of Dentistry, Dept. of Operative and Preventive Dentistry and Endodontics, Düsseldorf, Germany
,
Senay Tomruk
a   Heinrich-Heine-University, Medical Faculty, Centre of Dentistry, Dept. of Operative and Preventive Dentistry and Endodontics, Düsseldorf, Germany
,
Wolfgang H. M. Raab
a   Heinrich-Heine-University, Medical Faculty, Centre of Dentistry, Dept. of Operative and Preventive Dentistry and Endodontics, Düsseldorf, Germany
,
Ralf Janda
a   Heinrich-Heine-University, Medical Faculty, Centre of Dentistry, Dept. of Operative and Preventive Dentistry and Endodontics, Düsseldorf, Germany
› Institutsangaben
Weitere Informationen

Publikationsverlauf

Publikationsdatum:
30. September 2019 (online)

Auch verfügbar auf
  als PDF herunterladen Lizenzen und Reprints

Objectives: The purpose of this study was to evaluate flexural strengths, moduli, and maximum deflection of Clearfil AP-X (APX) and Ceram-X Mono (CXM) when cured with a quartz-tungsten halogen (QTH) or an LED-light (LED).

Methods: Specimens were made according to ISO 4049 and cured with QTH or LED for 10, 20 or 60 s. Flexural strength, modulus, and deflection were determined after 24 h water storage at 37°C and after thermocycling. Statistical significance was P<.05.

Results: Flexural strength did not depend on energy density or curing light and was significantly higher for APX than for CXM but decreased after thermocycling for both materials. Modulus and deflection depended on energy density. Modulus was significantly higher for APX than for CXM and increased for APX but decreased for CXM after thermocycling. Deflection decreased with increasing energy density and decreased after thermocycling. Though energy density did not influence flexural strength, it positively correlated with flexural modulus and negatively with maximum deflection.

Conclusions: Energy density did not influence flexural strength but modulus and deflection. Thermocycling affected all material properties. The LED was as effective as the QTH. (Eur J Dent 2010;4:183-191)

Keywords

Resin-based filling material - Mechanical properties - LED - Curing device - Curing time
 

  • References

  • 1 Leonard D, Charlton D, Roberts H, Cohen M. Polymerization efficiency of LED curing lights. J Esthet Restor Dent 2002; 14: 286-295
    CrossrefPubMedSuche in Google Scholar
  • 2 Uhl A, Mills RW, Vowles RW, Jandt KD. Knoop hardness depth profiles and compressive strength of selected dental composites polymerized with halogen and LED light curing technologies. J Biomed Mater Res 2002; 63: 729-738
    CrossrefPubMedSuche in Google Scholar
  • 3 Schneider LF, Consani S, Correr-Sobrinho L, Correr AB, Sinhoreti MA. Halogen and LED light curing of composite: temperature increase and Knoop hardness. Clin Oral Investig 2006; 10: 66-71
    CrossrefPubMedSuche in Google Scholar
  • 4 Yap AU, Soh MS, Han TT, Siow KS. Influence of curing lights and modes on cross-link density of dental composites. Oper Dent 2004; 29: 410-415
    PubMedSuche in Google Scholar
  • 5 Tsai PC, Meyers IA, Walsh LJ. Depth of cure and surface microhardness of composite resin cured with blue LED curing lights. Dent Mater 2004; 20: 364-369
    CrossrefPubMedSuche in Google Scholar
  • 6 Knezevic A, Tarle Z, Meniga A, Sutalo J, Pichler G. Influence of light intensity from different curing units upon composite temperature rise. J Oral Rehabil 2005; 32: 362-367
    CrossrefPubMedSuche in Google Scholar
  • 7 Knezevic A, Tarle Z, Meniga A, Sutalo J, Pichler G, Ristic M. Degree of conversion and temperature rise during polymerization of composite resin samples with blue diodes. J Oral Rehabil 2001; 28: 586-591
    CrossrefPubMedSuche in Google Scholar
  • 8 Uhl A, Volpel A, Sigusch BW. Influence of heat from light curing units and dental composite polymerization on cells in vitro. J Dent 2006; 34: 298-306
    CrossrefPubMedSuche in Google Scholar
  • 9 Campregher UB, Samuel SM, Fortes CB, Medina AD, Collares FM, Ogliari FA. Effectiveness of second-generation light-emitting diode (LED) light curing units. J Contemp Dent Pract 2007; 8: 35-42
    PubMedSuche in Google Scholar
  • 10 Hasler C, Zimmerli B, Lussi A. Curing capability of halogen and LED light curing units in deep class II cavities in extracted human molars. Oper Dent 2006; 31: 354-363
    CrossrefPubMedSuche in Google Scholar
  • 11 Uhl A, Mills RW, Rzanny AE, Jandt KD. Time dependence of composite shrinkage using halogen and LED light curing. Dent Mater 2005; 21: 278-286
    CrossrefPubMedSuche in Google Scholar
  • 12 Bala O, Olmez A, Kalayci S. Effect of LED and halogen light curing on polymerization of resin-based composites. J Oral Rehabil 2005; 32: 134-140
    CrossrefPubMedSuche in Google Scholar
  • 13 Fleming GJ, Khan S, Afzal O, Palin WM, Burke FJ. Investigation of polymerisation shrinkage strain, associated cuspal movement and microleakage of MOD cavities restored incrementally with resin-based composite using an LED light curing unit. J Dent 2007; 35: 97-103
    CrossrefPubMedSuche in Google Scholar
  • 14 Soh MS, Yap AU, Yu T, Shen ZX. Analysis of degree of conversion of LED and halogen lights using micro-Raman spectroscopy. Oper Dent 2004; 29: 571-577
    PubMedSuche in Google Scholar
  • 15 Beun S, Glorieux T, Devaux J, Vreven J, Leloup G. Characterization of nanofilled compared to universal and microfilled composites. Dent Mater 2007; 23: 51-59
    CrossrefPubMedSuche in Google Scholar
  • 16 Stahl F, Ashworth SH, Jandt KD, Mills RW. Light-emitting diode (LED) polymerisation of dental composites: flexural properties and polymerisation potential. Biomaterials 2000; 21: 1379-1385
    CrossrefPubMedSuche in Google Scholar
  • 17 Besnault C, Pradelle-Plasse N, Picard B, Colon P. Effect of a LED versus halogen light cure polymerization on the curing characteristics of three composite resins. Am J Dent 2003; 16: 323-328
    PubMedSuche in Google Scholar
  • 18 EN ISO 4049:2000 Dentistry -Polymer-based filling, restorative and luting materials.
  • 19 Price RB, Felix CA. Effect of delivering light in specific narrow bandwidths from 394 to 515nm on the micro-hardness of resin composites. Dent Mater 2009; 25: 899-908
    CrossrefPubMedSuche in Google Scholar
  • 20 Mobarak E, Elsayad I, Ibrahim M, El-Badrawy W. Effect of LED light-curing on the relative hardness of tooth-colored restorative materials. Oper Dent 2009; 34: 65-71
    CrossrefPubMedSuche in Google Scholar
  • 21 Gritsch K, Souvannasot S, Schembri C, Farge P, Grosgogeat B. Influence of light energy and power density on the microhardness of two nanohybrid composites. Eur J Oral Sci 2008; 116: 77-82
    CrossrefPubMedSuche in Google Scholar
  • 22 Silva CM, Dias KR. Compressive strength of esthetic restorative materials polymerized with quartz-tungsten-halogen light and blue LED. Braz Dent J 2009; 20: 54-57
    Suche in Google Scholar
  • 23 Kwon YH, Jeon GH, Jang CM, Seol HJ, Kim HI. Evaluation of polymerization of light-curing hybrid composite resins. J Biomed Mater Res B Appl Biomater 2006; 76: 106-113
    Suche in Google Scholar
  • 24 Janda R, Roulet JF, Latta M, Ruttermann S. The effects of thermocycling on the flexural strength and flexural modulus of modern resin-based filling materials. Dent Mater 2006; 22: 1103-1108
    CrossrefPubMedSuche in Google Scholar
  • 25 Pilato LA, Michno MJ. Advanced composite materials. Editor; Springer, New York: 1994
    Suche in Google Scholar
  • 26 Sambasivan S, Fischer DA, Shen MC, Hsu SM. Molecular orientation of ultrahigh molecular weight polyethylene induced by various sliding motions. J Biomed Mater Res B Appl Biomater 2004; 70: 278-285
    Suche in Google Scholar
  • 27 Edidin AA, Jewett CW, Kalinowski A, Kwarteng K, Kurtz SM. Degradation of mechanical behavior in UHMWPE after natural and accelerated aging. Biomaterials 2000; 21: 1451-1460
    CrossrefPubMedSuche in Google Scholar
  • 28 Teoh SH, Martin RL, Lim SC, Lee KH, Mok CK, Kwok WC. Delrin as an occluder material. ASAIO Trans 1990; 36: M417-421
    Suche in Google Scholar
  • 29 Kostoulas I, Kavoura VT, Frangou MJ, Polyzois GL. Fracture force, deflection, and toughness of acrylic denture repairs involving glass fiber reinforcement. J Prosthodont 2008; 17: 257-261
    CrossrefPubMedSuche in Google Scholar
  • 30 Uzun G, Keyf F. The effect of fiber reinforcement type and water storage on strength properties of a provisional fixed partial denture resin. J Biomater Appl 2003; 17: 277-286
    CrossrefPubMedSuche in Google Scholar
  • 31 Peutzfeldt A, Asmussen E. Resin composite properties and energy density of light cure. J Dent Res 2005; 84: 659-662
    Suche in Google Scholar
  • 32 Sideridou I, Tserki V, Papanastasiou G. Effect of chemical structure on degree of conversion in light-cured dimethacrylate-based dental resins. Biomaterials 2002; 23: 1819-1829
    CrossrefPubMedSuche in Google Scholar
  • 33 Peutzfeldt A. Resin composites in dentistry: the monomer systems. Eur J Oral Sci 1997; 105: 97-116
    CrossrefPubMedSuche in Google Scholar
  • 34 Owens BM, Rodriguez KH. Radiometric and spectrophotometric analysis of third generation light-emitting diode (LED) light-curing units. J Contemp Dent Pract 2007; 8: 43-51
    PubMedSuche in Google Scholar
  • 35 Wendl B, Droschl H, Kern W. A comparative study of polymerization lamps to determine the degree of cure of composites using infrared spectroscopy. Eur J Orthod 2004; 26: 545-551
    CrossrefPubMedSuche in Google Scholar
  • 36 Asmussen E, Peutzfeldt A. Flexural strength and modulus of a step-cured resin composite. Acta Odontol Scand 2004; 62: 87-90
    CrossrefPubMedSuche in Google Scholar
  • 37 Musanje L, Darvell BW. Polymerization of resin composite restorative materials: exposure reciprocity. Dent Mater 2003; 19: 531-541
    CrossrefPubMedSuche in Google Scholar
  • 38 Rodrigues Jr SA, Zanchi CH, Carvalho RV, Demarco FF. Flexural strength and modulus of elasticity of different types of resin-based composites. Braz Oral Res 2007; 21: 16-21
    PubMedSuche in Google Scholar
  • 39 Turssi CP, Ferracane JL, Ferracane LL. Wear and fatigue behavior of nano-structured dental resin composites. J Biomed Mater Res B Appl Biomater 2006; 78: 196-203
    Suche in Google Scholar
  • 40 Scientific Documentation Ceram-X Mono, DeTrey Dentsply GmbH, Constance, Germany. 2003
    Suche in Google Scholar
  • 41 Instructions for Use Ceram-X Mono, DeTrey Dentsply GmbH, Constance, Germany. 2003
    Suche in Google Scholar
  • 42 Soh MS, Yap AU. Influence of curing modes on crosslink density in polymer structures. J Dent 2004; 32: 321-326
    CrossrefPubMedSuche in Google Scholar