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Synthesis 1985; 1985(10): 935-937
DOI: 10.1055/s-1985-31390
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Synthesis of N-Alkyl-N-aryl- and N,N-Dialkyl-sulfamic Esters by Solid Liquid Phase Transfer Catalytic N-Alkylation of the Mono-N-substituted Esters

Padraig O. Burke* , William J. Spillane
  • *Chemistry Department, University College, Galway, Ireland
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Publication Date:
27 September 2002 (online)

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General, high-yield procedures for N-alkylation of esters of mono-N-substituted sulfamic acids involving reactions at ambient temperatures in the presence of a phase-transfer catalyst and excess alkylating agent have been developed.