Synthesis 1985; 1985(12): 1131-1133
DOI: 10.1055/s-1985-31450
communication
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.

Vacuum Gas/Solid N-Chlorination: Preparative Scale Synthesis of Volatile N-Chloramines

J. C. Guillemin* , J. M. Denis
  • *Laboratoire de Physicochimie Structurale III, Unité Associée au CNRS no 704, Université de Rennes I, Campus de Beaulieu, F-35042 Rennes Cedex, France
Further Information

Publication History

Publication Date:
27 September 2002 (online)

A simple method for the preparative scale synthesis of volatile chloramines free from impurities starting from the corresponding primary or secondary amine using N-chlorosuccinimide as chlorinating agent is described.