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Synthesis 1987; 1987(10): 896-899
DOI: 10.1055/s-1987-28113
DOI: 10.1055/s-1987-28113
paper
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Synthesis of Functionally Substituted α,β-Unsaturated Carbonyl Compounds
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Publication History
Publication Date:
12 September 2002 (online)
Epichlorohydrin and glycidol are transformed in a four step sequence into β-dimethylamino-α-phenylthio-substituted α,β-unsaturated carbonyl compounds 5, possessing differently O-protected oxymethyl substituents at the carbonyl group. These compounds are of value as intermediates in inverse-type hetero-Diels-Alder reactions.