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Synthesis 1987; 1987(12): 1092-1093
DOI: 10.1055/s-1987-28178
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Titanium Tetrachloride-Catalyzed Reaction of Diketene with Unsaturated Organosilanes. A Useful Synthesis of ß-Dicarbonyl Compounds

Masatomi Ohno* , Shotaro Matsuoka, Shoji Eguchi
  • *Institute of Applied Organic Chemistry, Faculty of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya 464, Japan
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Publication Date:
20 August 2002 (online)

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Allylsilane and silyl ketene acetal were acetoacetylated with diketene in the presence of titanium tetrachloride.