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Synthesis 1988; 1988(5): 366-369
DOI: 10.1055/s-1988-27575
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A Facile Synthesis of Alkyl Iodides and Deuterated Alkyl Iodides by Hydroiodination and Deuterioiodination of Olefins

Shinji Irifune* , Takao Kibayashi, Yasutaka Ishii, Masaya Ogawa
  • *Department of Applied Chemistry, Faculty of Engineering, Kansai University, Senriyama, Suita, Osaka 564, Japan
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Publication Date:
20 August 2002 (online)

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Chlorotrimethylsilane/sodium iodide in the presence of water has been found as facile method for the hydroiodination of olefins to alkyl iodides under mild conditions. This procedure has successfully been extended to the preparation of deuterated alkyl iodides by using deuterium oxide in place of water.