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Synthesis 1989; 1989(11): 855-856
DOI: 10.1055/s-1989-27409
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Functionalized Homocubanes: Oxidative Deiodination of Homocubyl Iodide. Synthesis of 4-Mesyloxy-, 4-Tosyloxy-, and 4-Chloro-1-bromopentacyclo[4.3.0.02,5.03,8.04,7]nonan-9-one Ethylene Acetal from the Corresponding 4-Iodo-1-bromohomocubyl with Hypervalent Iodine

Robert M. Moriarty* , Jaffar S. Khosrowshahi
  • *Department of Chemistry, University of Illinois at Chicago, P.O. Box 4348, Chicago, IL 60680, USA
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Publication Date:
02 May 2002 (online)

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4-Iodo-1-bromopentacyclo[4.3.0.02,5.03,8.04,7] nonan-9-one ethylene (1) undergoes substitution via a ligand exchange process.