A New Synthetic Method for β-Substituted γ-Butyrolactones via  Palladium-Catalyzed Reaction of 2-Butene-1,4-diol with Aryl and 1-Alkenyl Halides, and Subsequent Oxidation

Tadakatsu Mandai; Shun-ichi Hasegawa; Tadashi Fujimoto; Mikio Kawada; Junzo Nokami; Jiro Tsuji

doi:10.1055/s-1990-20993

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Synlett 1990; 1990(2): 85-86
DOI: 10.1055/s-1990-20993

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A New Synthetic Method for β-Substituted γ-Butyrolactones via Palladium-Catalyzed Reaction of 2-Butene-1,4-diol with Aryl and 1-Alkenyl Halides, and Subsequent Oxidation

Tadakatsu Mandai^* , Shun-ichi Hasegawa, Tadashi Fujimoto, Mikio Kawada, Junzo Nokami, Jiro Tsuji

^*Department of Applied Chemistry, Okayama University of Science, Ridai-cho, Okayama 700, Japan

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Publication Date:
08 March 2002 (online)

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The palladium-catalyzed reaction of 2-butene-1,4-diol with aryl and 1-alkenyl halides under phase-transfer conditions affords 4-substituted 2-hydroxytetrahydrofurans, which are oxidized to 4-substituted 2(3H)-dihydrofuranones (γ-butyrolactones).