Alkenyl Bromides by Brominative Deoxygenation of Ketones in One or Two Steps

Ulrich Von Roman; Jakob Ruhdorfer; Rudolf Knorr

doi:10.1055/s-1993-25986

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Synthesis 1993; 1993(10): 985-992
DOI: 10.1055/s-1993-25986

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Alkenyl Bromides by Brominative Deoxygenation of Ketones in One or Two Steps

Ulrich Von Roman^* , Jakob Ruhdorfer, Rudolf Knorr

^*Institute of Organic Chemistry, University of Munich, Karlstr. 23, D-80 333 Munich, Germany

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Publication Date:
29 April 2002 (online)

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The conversion of ketones into alkenyl bromides is accomplished in one or two steps by 2,2,2-tribromo-2,2-dihydro-1,3,2-benzodioxaphosphole or by the dibromomethyl methyl ether prepared therefrom. Investigations of the scope and limitations provide some hints for the preparative planning and improvement.