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Synthesis 1994; 1994(9): 926-930
DOI: 10.1055/s-1994-25606
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Synthesis of 4,5-Bis- and 4,4′,5,5′-Tetrakis(2-hydroxyethylthio) tetrathiafulvalene: The Assembly of Tris- and Pentakis(tetrathiafulvalene) Macromolecules

Gary J. Marshallsay* , Thomas K. Hansen, Adrian J. Moore, Martin R. Bryce, Jan Becher
  • *Department of Chemistry, University of Durham, Durham DH1 3LE, England
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Publication Date:
17 September 2002 (online)

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Efficient syntheses are reported of the novel pentakis- and tris(tetrathiafulvalene) derivatives 11 and 12, respectively, by esterification of tetraol and diol derivatives 8 and 10 with TTF-carbonyl chloride.