Simple Alternative Method for the Preparation of Bis(dimethylamino)methylene(trimethylsilyl)phosphane

Lothar Weber; O. Kaminski

doi:10.1055/s-1995-3867

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Synthesis 1995; 1995(2): 158
DOI: 10.1055/s-1995-3867

short paper

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Simple Alternative Method for the Preparation of Bis(dimethylamino)methylene(trimethylsilyl)phosphane

Lothar Weber^* , O. Kaminski¹

^*Fakultät für Chemie der Universität, Postfach 100131, D-33501 Bielefeld, Germany

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Publikationsdatum:
31. Dezember 2000 (online)

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Bis(dimethylamino)methylene(trimethylsilyl)phosphane is prepared in good yield by the reaction of the thiuronium salt [(Me₂N)₂CSMe]I with LiP(SiMe₃)₂ in 1,2-dimethoxyethane.

phosphaalkene - thiuronium iodide - lithium disilylphosphide - condensation