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Synlett 1995; 1995(1): 99-100
DOI: 10.1055/s-1995-4845
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A Novel Convenient One-pot Synthesis of N-Mono- and N,N-Di-Substituted Thioamides Mediated by 1-Trifluoromethylsulfonylbenzotriazole

Alan R. Katritzky* , Jean-Luc Moutou, Zhijun Yang
  • *Center for Heterocyclic Compounds, Department of Chemistry, University of Florida, Gainesville, FL 32611-7200, USA
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Publication Date:
31 December 2000 (online)

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Successive reactions of Grignard reagents with carbon disulfide, 1-trifluoromethylsulfonylbenzotriazole, and amines afford the corresponding N-mono- and N,N-di-substituted thioamides in good yields.

synthesis - thioamides - benzotriazole - Grignard - carbon disulfide