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Synlett 1995; 1995(7): 751-752
DOI: 10.1055/s-1995-5065
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Sodium Sulfide Adsorbed on Alumina as a Reagent for the Facile Synthesis of 2,11-Dithia[3.3]metacyclophanes

Graham J. Bodwell* , Tom J. Houghton, Holly E. Koury, Bala Yarlagadda
  • *Department of Chemistry, Memorial University of Newfoundland, St. John’s, Newfoundland, Canada A1B 3X7
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Publication Date:
31 December 2000 (online)

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2,11-Dithia[3.3]metacyclophanes without internal substituents can be prepared rapidly, easily and in moderate yield by using sodium sulfide adsorbed on alumina (Na2S/Al2O3).

Cyclophanes - Sodium Sulfide - Alumina