The First Example of Nitrone Cycloaddition with [60]Fullerene. A Facile Access to Isoxazoline-Fused C60 with Nitroalkanes

Masatomi Ohno; Arihiro Yashiro; Shoji Eguchi

doi:10.1055/s-1996-5622

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Synlett 1996; 1996(9): 815-816
DOI: 10.1055/s-1996-5622

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The First Example of Nitrone Cycloaddition with [60]Fullerene. A Facile Access to Isoxazoline-Fused C₆₀ with Nitroalkanes

Masatomi Ohno, Arihiro Yashiro, Shoji Eguchi^*

^*Department of Molecular Design and Engineering, Graduate School of Engineering, Nagoya University, Chikusa, Nagoya 464-01, Japan

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Publication Date:
31 December 2000 (online)

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C₆₀ underwent smooth 1,3-dipolar cycloaddition reaction with N-silyloxynitrones formed from nitroalkanes and Me₃SiCl/Et₃N to give isoxazoline-fused C₆₀ derivatives after acid treatment.

fullerene - nitrone - 1,3-dipolar cycloaddition - isoxazolidine - isoxazoline