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Synlett 1997; 1997(10): 1190-1192
DOI: 10.1055/s-1997-975
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1,4,8,11-Tetraazabicyclo[9.3.1]pentadecanes: Synthesis and Use of a New Strategy for the Selective cis-N4,N8-Difunctionalization of Cyclam Derivatives

Roger Guilard1 , Alla G. Bessmertnykh2 , Irina P. Beletskaya3
  • 1Laboratoire d’Ingénierie Moléculaire pour la Séparation et les Applications des Gaz (L.I.M.S.A.G.), U.M.R. n° 5633, Univesité de Bourgogne, Faculté des Sciences Gabriel, 21100 Dijon, France, Fax 33 3 80 39 61 17; rguilard@u-bourgogne.fr
  • 2Laboratoire d’Ingénierie Moléculaire pour la Séparation et les Applications des Gaz (L.I.M.S.A.G.), U.M.R. n° 5633, Univesité de Bourgogne, Faculté des Sciences Gabriel, 21100 Dijon, France
  • 3Department of Chemistry, Moscow State University, Moscow, SU-119899, Russia, Fax 7 095 938 18 44; beletska@org.chem.msu.su
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Publication History

Publication Date:
31 December 2000 (online)

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A new efficient route to derivatives of 1,4,8,11-tetraazabicyclo[9.3.1]pentadecane 2 and their use in a procedure of selective N4,N8-difunctionalization of cyclam is reported.

cyclam protection - diethylaminotrialkylstannane - 1,4,8,11-tetraazabicyclo[9.3.1]pentadecane