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Synthesis 1999; 1999(5): 803-810
DOI: 10.1055/s-1999-3473
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A Novel Tetrathiafulvalene Building Block

Jan Oskar Jeppesen* , Kazuo Takimiya, Niels Thorup, Jan Becher
  • *Department of Chemistry, University of Odense, Campusvej 55, DK-5230 Odense M, Denmark; Fax +45(66)15 87 80; E-mail: jbe@chem.ou.dk
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Publication History

Publication Date:
31 December 1999 (online)

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Efficient synthesis of a novel tetrathiafulvalene building block, 2,3-bis(2-cyanoethylthio)-6,7-bis(thiocyanatomethyl)tetrathiafulvalene (7) useful for stepwise and asymmetrical bis-functionalization is reported.

tetrathiafulvalene building block - orthogonal sets of protection groups - stepwise and asymmetrical bis-functionalization - thiocyanatomethyl - bromomethyl