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Synthesis 1999; 1999(5): 844-848
DOI: 10.1055/s-1999-3477
DOI: 10.1055/s-1999-3477
paper
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A General Synthesis of Thiophosphates Containing an α,β-Unsaturated Carbonyl Moiety
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Publikationsverlauf
Publikationsdatum:
31. Dezember 1999 (online)
![](https://www.thieme-connect.de/media/synthesis/199905/lookinside/thumbnails/10.1055-s-1999-3477-1.jpg)
The O-silylated dienolates of α,β-unsaturated ketones and aldehydes can be thiophosphorylated using O,O-dialkylchlorothiophosphonates and O,O-dialkylbromodithiophosphonates to give a new class of compounds thio- and dithiophosphates 1-4 in high yield.
unsaturated ketones - aldehydes - O-silylated dienolates - thiophosphates - dithiophosphates