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Synthesis 1999; 1999(1): 64-65
DOI: 10.1055/s-1999-3695
short paper
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A Practical Method for the Preparation of Nitriles from Primary Amides Under Non-Acidic Conditions

D. Subhas Bose* , B. Jayalakshmi
  • *Organic Chemistry Division III, Indian Institute of Chemical Technology, Hyderabad 500 007, India; Fax +91-40-7 17 33 87/7 17 37 57; E-mail: root@csiict.ren.nic.in
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Publikationsdatum:
31. Dezember 1999 (online)

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In order to establish a mild conversion method of primary amides to nitriles, various types of carboxamides were treated with trifluoromethanesulfonic anhydride and triethylamine, as a dehydrating agent to obtain the desired nitriles in 84-95% yields.

trifluoromethanesulfonic anhydride - carboxamides - dehydration

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