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Synthesis 2000; 2000(11): 1539-1542
DOI: 10.1055/s-2000-7597
DOI: 10.1055/s-2000-7597
paper
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A Mild One-Pot Procedure for the Polynitration of Activated Arenes. Convenient Preparation of Dinitro- and Trinitrodialkoxybenzenes
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Publikationsverlauf
Publikationsdatum:
31. Dezember 2000 (online)
![](https://www.thieme-connect.de/media/synthesis/200011/lookinside/thumbnails/10.1055-s-2000-7597-1.jpg)
When first treated with an excess of nitrogen dioxide alone and then in the presence of ozone at low temperature, dialkoxybenzenes are smoothly and stepwise polynitrated in a one-pot manner to afford the corresponding dinitro or trinitro derivatives in good yield.
dialkoxybenzenes - nitration - polynitro compounds - nitrogen dioxide - ozone