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Synlett 2001; 2001(7): 1101-1104
DOI: 10.1055/s-2001-15164
DOI: 10.1055/s-2001-15164
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Parallel Synthesis of Oligosaccharide Conjugated Enediynes onto Silyl-linked Solid-Support
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Publication History
Publication Date:
31 December 2001 (online)
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A solid-phase synthesis of enediyne molecules containing a sugar moiety is reported. Polymer-supported (2-mercaptoethyl)glycosides linked through a trialkylsilane linker were coupled to a bromoacetate on an enediyne by S-alkylation. After simple washing of the polymer, mild acid treatment, and evaporation, the desired oligosaccharide conjugated enediynes were isolated in pure form in parallel fashion.
solid-phase synthesis - oligosaccharides - coupling - thiols