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Synlett 2001; 2001(8): 1221-1224
DOI: 10.1055/s-2001-16056
DOI: 10.1055/s-2001-16056
letter
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Synthesis of a Model System for the Macrocyclic Subunit of the Oximidines
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Publikationsverlauf
Publikationsdatum:
31. Dezember 2001 (online)
![](https://www.thieme-connect.de/media/synlett/200108/lookinside/thumbnails/10.1055-s-2001-16056-1.jpg)
Cross-coupling reaction of aryl triflate 1 and vinyl stannane 13 provided salicylic acid derivative 15. This compound was converted to the dihydroxy acid 16, which provided in a size-selective macrolactonization the two macrolides 17 and 18 in a ratio of 60 : 40. Compound 17 is a model of the macrocyclic core of the oximidines.
arylations - dihydroxylations - hydrostannations - macrocycles - Stille reaction