Synthesis

Category: addenda and errata

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Issue 03/2012

Cyclic Aromatic Analogues of the Hendrickson Reagent; NMR Studies and Electrophilic Properties

Issue 01/2012

Synthesis of 1-Chloroalkynes from Alkynylsilanes Using Trichloroisocyanuric Acid as Chlorinating Agent
tert-Butoxide-Assisted Amidation of Esters under Green Conditions

Issue 24/2011

Microwave-Assisted Solvent-Free Diels-Alder Reaction - A Fast and Simple Route to Various 5,6-Substituted Norbornenes and Polychlorinated Norbornenes

Issue 23/2011

Regioselective Syntheses of Substituted Pyridines and 2,2′-Bipyridines by Cobalt-Catalyzed [2+2+2] Cycloaddition of α,ω-Diynes with Nitriles

Issue 21/2011

Mechanistic Studies on a New Catalyst System (CuI-NaHSO4×SiO2) Leading to the One-Pot Synthesis of Imidazo[1,2-a]pyridines from Reactions of 2-Aminopyridines, Aldehydes, and Terminal Alkynes

Issue 19/2011

Synthesis and Structure of Fluorescent Chelate Boron Complexes of 4-Anilinomethylidene-1-benzazepine-2,5-dione Ligands

Issue 16/2011

Mild Conditions for Copper-Catalyzed N-Arylation of Imidazoles

Issue 13/2011

RuO4-Catalyzed Oxidation Reactions of N-Alkylisoxazolino-2-azanorbornane Derivatives: An Expeditious Route to Tricyclic γ-Lactams

Issue 11/2011

Reactions of Unsaturated Azides; Part 27: Synthesis of 1,4-Diazidobuta-1,3-dienes
Ultrasound-Promoted Formation of Isopentenyl Alcohol Dianion: Straightforward Synthesis of Perhydrofuro[2,3-b]furans
Inexpensive Copper/Iron-Cocatalyzed Reactions

Issue 08/2011

Thermal and Microwave-Assisted Rapid Syntheses of Substituted Imidazo[1,2-a]pyridines Under Solvent- and Catalyst-Free Conditions
Stereoselective Synthesis of Stagonolide G from d-Mannitol

Issue 05/2011

A Mild and Efficient Synthesis of Buta-1,3-dienes Substituted with a Terminal Pentafluoro-λ6-sulfanyl Group
Ecofriendly Iodination of Activated Aromatics and Coumarins Using Potassium Iodide and Ammonium Peroxodisulfate

Issue 02/2011

Synthesis of 3-Heteroaryloxindoles through t-BuOCl-Mediated Oxidation of 3-Heteroarylindoles

Issue 22/2010

An Improved Synthesis of 1,4,7-Triazacyclononanes (tacns) and 1,4,7,10-Tetraazacyclododecanes (cyclens)

Issue 21/2010

Stereoselective Total Synthesis of Obolactone via Prins Cyclization
Expeditious Synthesis of Trifluoromethylated Heterocycles: Noncatalytic 1,3-Dipolar Cyclization of Azomethine Imines with (α-Trifluoromethyl)acrylates
Synform

Issue 19/2010

Synthesis of 1,5,6,7-Tetrahydro-4H-pyrazolo[4,3-c]pyridin-4-ones as Conformationally Constrained Pyrazole Analogues of Histamine

Issue 14/2010

Studies on the Chemistry of 2-[3-(2-Nitrophenyl)-2-oxopropyl]benzaldehydes: Novel Syntheses of 5H-Benzo[b]carbazole-6,11-diones and Indolo[1,2-b]- isoquinoline-6,11-diones
A Flexible Synthesis of Indoles from ortho-Substituted Anilines: A Direct Synthesis of Isocryptolepine

Issue 12/2010

Synthesis of Halogenated Carboxylic Acids and Amino Acids

Issue 08/2010

A Concise Synthesis of (S)-2-(Fluorodiphenylmethyl)pyrrolidine: A Novel Organocatalyst for the Stereoselective Epoxidation of α,β-Unsaturated Aldehydes

Issue 04/2010

‘Ligand-Free-Like’ CuCl-Catalyzed Atom Transfer Radical Cyclization of N-Substituted N-Allyl Polychloroamides to γ-Lactams

Issue 03/2010

A Facile Chiral Pool Synthesis of (S)-6-Nitroindoline-2-carboxylic Acid from
l-Phenylalanine

Issue 02/2010

O,S-Dimethyl Carbonodithioate as a Phosgene Substitute for the Preparation of
S-Methyl Alkylcarbamothioates and Dialkylcarbamothioates

Issue 01/2010

Synthesis of 1,11-Dihydro-2H-[1,3]oxazolo[4′,5′:5,6]indeno[1,2-b]quinolin-2-ones with Potential Topoisomerase I Inhibitory Activity

Issue 23/2009

Regioselective, One-Pot Syntheses of Symmetrically and Unsymmetrically Halogenated 2′,6′-Bispyrazolylpyridines

Issue 22/2009

Total Synthesis of (±)-Petasitolone and (±)-Fukinone

Issue 21/2009

A New Approach to Methoxyisatins Leading to the Total Synthesis of Ophiuroidine and Other Hydroxytryptanthrins
A Straightforward Synthesis of 2-(1-Vinyl-1H-pyrrol-2-yl)-1H-benzimidazoles from 1-Vinyl-1H-pyrrole-2-carbaldehydes and o-Phenylenediamine

Issue 18/2009

Transition-Metal-Catalyzed Enantioselective Synthesis of Compounds with Non-Centrochirality

Issue 17/2009

Enantioselective Aldol Reaction of Tetrasubstituted Ketene Silyl Acetals with Achiral Aldehydes for the Construction of Asymmetric Tertiary Alcohols: An Application for the Divergent Total Syntheses of Buergerinins F and G

Issue 16/2009

Iodogen: A Novel Reagent for the Oxidation of Urazoles under Heterogeneous Conditions

Issue 11/2009

Facile Synthesis of Fluorinated 1-Desazapurines

Issue 10/2009

Convenient Methods for Synthesis of C2-Symmetric Diphenyltetrahydro­thiophenes

Issue 09/2009

Novel Synthesis of Naturally Occurring Pulvinones: A Heck Coupling, Transesterification, and Dieckmann Condensation Strategy

Issue 05/2009

Reactivity of 2-Halo-2H-azirines. Part II. Thermal Ring Expansion Reactions: Synthesis of 4-Haloisoxazoles

Issue 03/2009

Synthesis and Olfactory Evaluation of (4aR*,8aR*)-1,1,8a-Trimethyl­-decahydronaphthalen-4a-ol: A cis-Decalol Intersection Structure of (-)-Patchoulol and (5R*,6S*)-1,1,6-Trimethylspiro[4.5]decan-6-ol
Efficient Catalytic Activity of Copper/Aluminum Hydrotalcite in Diaryl Ether Synthesis

Issue 20/2008

Palladium-Catalyzed Synthesis of 3-Indolecarboxylic Acid Derivatives
Gold-Catalysis: Reactions of Furandialkynes

Issue 13/2008

Yamazaki, Yukiyoshi; Araki, Takaaki; Koura, Minoru; Shibuya, Kimiyuki: Enantioselective Synthesis of the PPARα Agonist (R)-K-13675 via (S)-2-Hydroxybutyrolactone

Issue 12/2008

Srihari, Pabbaraja; Reddy, Joolakanti Shyam Sunder; Mandal, Satadru Sekhar; Satyanarayana, Kamani; Yadav, Jhillu Singh: PMA-Silica Gel Catalyzed Propargylation of Aromatic Compounds with Arylpropargyl Alcohols under Solvent-Free Conditions

Issue 08/2008

Majumdar, Krishna C.; Chattopadhyay, Buddhadeb: Amino-Claisen versus Oxy-Claisen Rearrangement: Regioselective Synthesis of Pyrrolocoumarin Derivatives

Issue 07/2008

Chaturvedi, Devdutt; Mishra, Nisha; Mishra, Virendra: An Efficient, One-Pot Synthesis of S-Alkyl Thiocarbamates from the Corresponding Thiols Using the Mitsunobu Reagent

Issue 14/2007

Waldvogel, Siegfried: Book Review
Cyclodextrins and Their Complexes: Chemistry, Analytical Methods, Applications (Helena Dodziuk, Ed.)
Sarang, Prajakta S.; Yadav, Arun A.; Patil, Prashant S.; Krishna, Urlam Murali; Trivedi, Girish K.; Salunkhe, Manikrao M.: Synthesis of Advanced Intermediates of Lennoxamine Analogues

Issue 10/2007

Ward, Dale E.; Rasheed, M. Abdul; Gillis, H. Martin; Beye, Garrison E.; Jheengut, Vishal; Achonduh, George T.: Simple and Efficient Preparation of Reagents for Thiopyran Introduction: Methyl Tetrahydro-4-oxo-2H-thiopyran-3-carboxylate, Tetrahydro-4H-thiopyran-4-one, and 3,6-Dihydro-4-trimethylsilyloxy-2H-thiopyran

Issue 04/2007

Ma, Guang-Ning; Zhang, Yun-Peng; Shi, Min: l-Proline Diamides with an Axially Chiral Binaphthylene Backbone as Efficient­ Organocatalysts for Direct Asymmetric Aldol Reactions: The Effect of Acetic Acid
Winter, Andreas; van den Berg, Antje M. J.; Hoogenboom, Richard; Kickelbick, Guido; Schubert, Ulrich S.: A Green and Straightforward Synthesis of 4′-Substituted Terpyridines

Issue 24/2006

Korn, Tobias J.; Schade, Matthias A.; Cheemala, Murthy N.; Wirth, Stefan; Guevara, Simon A.; Cahiez, Gérard; Knochel, Paul: Cobalt-Catalyzed Cross-Coupling Reactions of Heterocyclic Chlorides with Arylmagnesium Halides and of Polyfunctionalized Arylcopper Reagents with Aryl Bromides, Chlorides, Fluorides and Tosylates

Issue 19/2006

Rahaim Jr, Ronald J.; Maleczka Jr, Robert E.: Palladium-Catalyzed Silane/Siloxane Reductions in the One-Pot Conversion of Nitro Compounds into Their Amines, Hydroxylamines, Amides, Sulfonamides, and Carbamates
Malhas, Rana N.; Ibrahim, Yehia A.: Synthesis of Olefinic Crown Diamides and their Conversion into Pyrazolino Macrocycles: Promising Photoluminescent Crown Compounds

Issue 18/2006

Ziessel, Raymond; Weibel, Nicolas; Charbonnière, Loïc J.: Stepwise Construction of Polysubstituted Phenanthroline-Based Glutamate Pockets for Lanthanide Complexation

Issue 14/2006

Roy, Ashim; Achari, Basudeb; Mandal, Sukhendu B.: A Short and Simple Synthesis of 1-Deoxynojirimycin Derivatives from d-Glucose

Issue 07/2006

Roy, Amrendra K.; Pathak, Richa; Yadav, Gaya P.; Maulik, Prakas R.; Batra, Sanjay: Neighboring-Group Effect: DBU-Promoted Ring Transformation of Substituted­ Isoxazoles to Substituted Pyrroles

Issue 18/2005

Gogritchiani, Eliso; Niebler, Sandra; Egner, Nicole; Wörner, Michael; Braun, André M.; Young, Tanya; Gupta, Prachi; Shi, Aibin; Bossmann, Stefan H.: Synthesis of Organic Thiosulfates Tailored for the Electrochemical Deposition of ‘Self-Assembled Monolayers’ at Gold Surfaces

Issue 16/2005

Singh, Ram; Geetanjali: Synthesis of Selected Novel Covalently Linked Flavoquinolones

Issue 15/2005

Porto, Ricardo S.; Vasconcellos, Mario L. A. A.; Ventura, Elizete; Coelho, Fernando: Diastereoselective Epoxidation of Allylic Diols Derived from Baylis-Hillman Adducts

Issue 13/2005

Hübner, Sandra; Neumann, Helfried; Wangelin, Axel Jacobi; Klaus, Stefan; Strübing, Dirk; Klein, Holger; Beller, Matthias: Efficient One-Pot Synthesis of Substituted 1-Acylaminocyclohex-2-enes

Issue 10/2005

Sigmund, Duanne; Schiesser, Carl H.; Wille, Uta: Alkoxyl Radicals as O-Synthons in Self-Terminating Radical Oxygenations: An Experimental and Theoretical Study

Issue 05/2005

Zhang, Guolin: Efficient Protocol for the Phosphine-Free Suzuki-Miyaura Reaction Catalyzed by Palladium on Carbon at Room Temperature

Issue 04/2005

Zaleska, Barbara; Trzewik, Bartosz; Stodolak, Ewa; Grochowski, Jacek; Serda, Paweł; Serda, Pawe: One-Pot Synthesis of 3,4-Dihydro-2H-pyrido[1,2-a][1,3,5]triazin-2-one Derivatives from N-(2′-Pyridinyl)benzoylacetamide and Nitrosobenzenes

Issue 01/2005

Shi, Enxue; Pei, Chengxin: Pseudohalogenation of Phosphites

Issue 17/2004

Budynina, Ekaterina M.; Averina, Elena B.; Ivanova, Olga A.; Yashin, Nikolai V.; Kuznetsova, Tamara S.; Zefirov, Nikolai S.: The First Synthesis of 1,1-Dinitrocyclopropane

Issue 12/2004

Paul, Satya; Gupta, Monika: Selective Fries Rearrangement Catalyzed by Zinc Powder

Issue 11/2004

Lin, C.; Fu, H.; Tu, G.; Zhao, Y.: Synthesis of AZT/d4T Boranophosphates as Anti-HIV Prodrug Candidates

Issue 10/2004

Yus, Miguel; Moreno, Benjamín; Foubelo, Francisco; Yus, M.; Moreno, B.; Foubelo, F.: Reductive Ring Opening of Oxygen-Containing Benzo-Fused Heterocycles by an Arene-Catalysed Lithiation
Kudyba, Iwona; Raczko, Jerzy; Jurczak, Janusz; Kudyba, I.; Raczko, J.; Jurczak, J.: Simple and Efficient Syntheses of N-Glyoxyloyl-7,7-dimethylnorbornane-(1S,2R)-oxazolidinone and Its Thio Derivative - Useful Chirons for Diastereoselective Reactions

Issue 07/2004

Palećek, Jiří; Paleta, Oldřich: Novel and Convenient Aldolisation of Methyl 3,3,3-Trifluoropyruvate Using Enamines Instead of Ketones

Issue 05/2004

Bravin, Fabio Massimo; Busnelli, Gilberto; Colombo, Matteo; Gatti, Francesco; Manzoni, Leonardo; Scolastico, Carlo; Bravin, F. M.; Busnelli, G.; Colombo, M.; Gatti, F.; Manzoni, L.; Scolastico, C.: Synthesis of Conformationally Restricted and Optically Pure Analogues of Serine­-Proline Dipeptide via Aldol Condensation