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Synlett 2023; 34(15): 1777-1780
DOI: 10.1055/s-0042-1751441
DOI: 10.1055/s-0042-1751441
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Taming SbH3: A Simple and Safe Approach to Using Stibane in Synthesis on a Laboratory Scale
We are grateful to the Deutsche Forschungsgemeinschaft for financial support.
Abstract
Herein, we present a simple, inexpensive, and readily accessible apparatus for the safe and clean preparation, isolation, and conversion of stibane (SbH3). In this setup, only typical standard glassware and fabric tubes are used. The pure stibane can be obtained in very good yields with very little expenditure of time.
Supporting Information
- Supporting information for this article is available online at https://doi.org/10.1055/s-0042-1751441.
- Supporting Information
Publication History
Received: 02 February 2023
Accepted after revision: 20 March 2023
Article published online:
18 April 2023
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