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Synlett 1990; 1990(8): 487-489
DOI: 10.1055/s-1990-21138
DOI: 10.1055/s-1990-21138
letter
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Azidobromination of Alkenes with Azidotrimethylsilane/N-Bromosuccinimide1
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Publikationsverlauf
Publikationsdatum:
08. März 2002 (online)
A very efficient azidobromination of alkenes to give ß-bromoalkyl azides using the superacidic perfluororesinsulfuric acid (Nafion-H®) catalyzed reaction of N-bromosuccinimide and azidotrimethylsilane in dichloromethane/nitromethane (3:1 by volume) is described.