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Synlett 1996; 1996(9): 885-886
DOI: 10.1055/s-1996-5613
DOI: 10.1055/s-1996-5613
letter
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An Extremely Mild, Convenient Procedure for the Reduction of Sulfoxides to Thioethers
Further Information
Publication History
Publication Date:
31 December 2000 (online)
![](https://www.thieme-connect.de/media/synlett/199609/lookinside/thumbnails/10.1055-s-1996-5613-1.jpg)
Treatment of sulfoxides with acetic anhydride or N,N-dimethylcarbamoyl chloride (2 mol equiv)/DMAP (0.1 mol equiv)/activated zinc (10 mol equiv) in CH2Cl2 or acetonitrile at room temperature has been shown to provide the corresponding reduction products, thioethers, in good to excellent yields.
reduction - sulfoxides - acetic anhydride - activated zinc - 1,2-dithiin monosulfoxide