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Synlett 1997; 1997(9): 1096-1098
DOI: 10.1055/s-1997-1525
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A Short Synthetic Route to Novel, Highly Soluble 3,8-Dialkyl-4,7-dibromo-1,10-phenanthrolines

Michael Schmittel* , Horst Ammon
  • *Institut für Organische Chemie der Universität Würzburg, Am Hubland, D-97074 Würzburg, Germany, FAX: Int +49 931 888 4606, e-mail: mjls@chemie.uni-wuerzburg.de
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Publication Date:
31 December 2000 (online)

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A short and convenient synthesis of highly soluble 3,8-dialkyl-4,7-dibromo-1,10-phenanthrolines is described. These compounds are versatile key building blocks for the preparation of macrocyclic oligophenanthrolines with exo-coordination sites.

phenanthroline - cyclization - bromination - Heck reaction