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Synlett 1997; 1997(8): 915-916
DOI: 10.1055/s-1997-971
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A Simple Synthesis of β-Amino Sulfides

Hiroyuki Ishibashi* , Masayuki Uegaki, Manami Sakai
  • *Faculty of Pharmaceutical Sciences, Kanazawa University, Takara-machi, Kanazawa 920, Japan, Fax +81(76)234-4476; E-mail: isibasi@dbs.p.kanazawa-u.ac.jp
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Publication Date:
31 December 2000 (online)

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Thiols reacted with 2-oxazolidinones in the presence of alkoxides to give β-amino sulfides in high yields. The method was applied to the synthesis of 5,6-dihydro-1,4-thiazin-3(2H)-ones.

aminoethylation - β-amino sulfide - 2-oxazolidinone - 5,6-dihydro-1,4-thiazin-3(2H)-one