Synlett

Issue 08 · August 1997

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863
Nemoto, Hideo; Fukumoto, Keiichiro: A Novel Domino Route to Chiral Cyclobutanones and its Function as Cornerstone in the Synthesis of Versatile Natural Products

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876
Iqbal, Javed; Mukhopadhyay, Manoj; Mandal, Ajay K.: Cobalt Catalyzed Organic Transformations: Highly Versatile Protocols for Carbon-Carbon and Carbon-Heteroatom Bond Formation

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887
Shimizu, Isao; Fujita, Munetsugu; Nakajima, Takayuki; Sato, Tadashi: Facile Synthesis of Keto Nitriles by Cu(II)-Promoted Photooxidative Cleavage of Cyclic Olefins

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889
Yu, Chan-Mo; Choi, Ha-Soon; Yoon, Sook-Kyung; Jung, Won-Hyuk: Effects of Subjoin Lewis Acid on the Catalytic Asymmetric Allylic Transfer Reactions of Aldehydes Promoted by BINOL-Ti(IV) Complex

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891
Yang, De-Yu; Huang, Xian: The Hydroboration-Iodination of Dialkylselenoacetylenes to Vinylic Diselenides

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893
Wessig, Pablo; Schwarz, Jutta: A Convenient One-Pot Conversion of N-Boc-β-Aminoalcohols into N-Boc-Aziridines

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895
May, Paul D.; Larsen, Scott D.: Preparation of Novel 6-Substituted-4-Hydroxy-2H-Pyran-2-one-3-Carboxamides and Esters via Palladium-Catalyzed Cross-Coupling Methodology

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897
Bonhôte, Pierre; Wrighton, Mark S.: Facile Synthesis of Tetrapyrido[2,3-a:3',2'-c:2",3"-h:3'",2'"-j]phenazine

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899
Yasuda, Minoru; Ide, Mitsuaki; Matsumoto, Yuka; Nakata, Masaya: Enantiospecific Synthesis of the 14-Memberes Diene Unit of methyl Sarcophytoate

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903
Schmidt, Wolfgang; Montforts, Franz-Peter: Synthesis of a Novel Enantiomerically Pure Chlorin as a Potential Subunit for an Artificial Photosynthetic Reaction Center

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905
Cossy, Janine; Dumas, Cécile; Pardo, Domingo Gomez: Synthesis of (-)-Pseudoconhydrine through Ring Enlargement of a L-Proline Derivative

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907
Yokoyama, Yasuo; Mochida, Kunio: Chemoselective Trifluoromethylation of Methyl Esters Using an Et₃GeNa/C₆H₅SCF₃ Combination: Efficient Synthesis of Trifluoromethyl Ketones

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909
Mittra, Asmita; Yamashita, Masayuki; Kawasaki, Ikuo; Murai, Hiromichi; Yoshioka, Tomomichi; Ohta, Shunsaku: A Useful Oxidation Procedure for the Preparation of 3-Alkanoyltetronic Acids

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911
Yoda, Hidemi; Nakajima, Tomohito; Takabe, Kunihiko: Stereocontrolled Synthesis of a Trihydroxylated Indolizidine Alkaloid, 1-Deoxycastanospermine

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913
Poignant, Géraldine; Martin, Françoise; Guerchais, Véronique: Activation of 2-Alkyn-1-ols by [Fe(C₅Me₅)(CO)₂]⁺: New Route to α,β-Unsaturated Acyl Complexes

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915
Ishibashi, Hiroyuki; Uegaki, Masayuki; Sakai, Manami: A Simple Synthesis of β-Amino Sulfides

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917
Caputo, Romualdo; Guaragna, Annalisa; Pedatella, Silvana; Palumbo, Giovanni: Mild and Regiospecific Phosphorylation of Nucleosides

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919
Blake, Alexander J.; Westaway, Susan M.; Simpkins, Nigel S.: The Enantioselective Conversion of Three-Membered Ring Sulfoxides (Episulfoxides) into Alkenyl Sulfoxides using Chiral Lithium Amide Bases

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921
Kaczmarczyk, Grzegorz; Joczyk, Andrzej: Chloromethyl(dimethyl)sulfonium Trifluoromethanesulfonate - The Reagent for Preparation of Acetals of 2-Hydroxyaldehydes from Ketones under Basic Conditions

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923
Cainelli, Gianfranco; DaCol, Marco; Galletti, Paola; Giacomini, Daria: Ruthenium Catalyzed Oxidation of 3-Amino-β-Lactams

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925
Knölker, Hans-Joachim; Braxmeier, Tobias: Isocyanates, Part 4. Convenient Phosgene-Free Method for the Synthesis and Derivatization of Enantiopure α-Isocyanato Carboxylic Acid Esters

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929
Khlebnikov, Alexander F.; Novikov, Mikhail S.; Kostikov, Rafael R.: A Facile Synthesis of New Ketenimine Derivatives of α-Amino Acids

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931
Renaud, Jean-Luc; Petit, Marc; Aubert, Corinne; Malacria, Max: Synthetic Usefulness of the Cobalt(I)-Mediated Ene Type Reaction for the Diastereoselective Construction of Bicyclo[n.3.0]derivatives

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933
Yanagisawa, Akira; Nakatsuka, Yoshinari; Nakashima, Hiroshi; Yamamoto, Hisashi: Asymmetric γ-Selective Pentadienylation of Aldehydes Catalyzed by BINAP•Ag(I) Complex

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935
Harwood, Laurence M.; Hamblett, Giles; Jiménez-Díaz, Antonio I.; Watkin, David J.: Enantiomerically Pure 3-Substituted 2-Phenylprolines by Caesium Fluoride/Tetramethoxysilane Mediated 1,4-Addition of 3(S)-5(R)-Diphenylmorpholin-2-one to Acrylates

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939
Kodra, Janos T.; Benner, Steven A.: Synthesis of an N-Alkyl Derivative of 2'-Deoxyisoguanosine

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941
Arcadi, Antonio: Regio and Stereoselective Synthesis of (E)-4-Arylidene/alkenylidene-3-tosyloxazolidin-2-ones through Palladium-Catalyzed Reactions of Aryl Iodides/Vinyl Triflates with Propargyl Tosylcarbamates

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944
Bouyssi, Didier; Cavicchioli, Marcello; Balme, Geneviève: Palladium-Catalyzed Synthesis of Stereodefined 4-Arylidene-3 Tosyloxazolidin-2-ones from 2-Propynyl Tosylcarbamates and Unsaturated Halides (or Triflate)

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947
Kim, Sunggak; Cheong, Jae Ho: Efficient Synthesis of dl-Zizaene Sesquiterpenes via Tandem Radical Cyclizations of N-Aziridinylimines

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950
Kim, Sunggak; Lee, Tai Au: Facile Generation of Alkyl, Aminyl, and Alkoxy Radicals from Se-Phenyl Benzoselenohydroximate Derivatives

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953
Banwell, Martin G.; Gable, Robert W.; Greenwood, Richard J.; Lambert, John N.; Mackay, Maureen F.; Walter, Justine M.: Ring-fused gem-Dibromocyclopropanes as Precursors to "Tunable" Molecular Clefts Possessing Convergent Functional Groups

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956
Yanagisawa, Akira; Watanabe, Tsuyoshi; Kikuchi, Tetsuo; Kuribayashi, Takeshi; Yamamoto, Hisashi: Diastereoselective Protonation of Chiral Enolate with Chiral Imides

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959
Cacchi, Sandro; Fabrizi, Giancarlo; Carangio, Antonella: Functionalised Pyrazoles through a Facile One-Pot Procedure from N-Tosyl-N-propargyl-hydrazine and Aryl Iodides or Vinyl Triflates

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962
Fujiwara, Tooru; Tsuruta, Yumiko; Arizono, Ko-ichi; Takeda, Takeshi: Oxidative Cleavage of vic-Diols Using Copper(II) Bromide-Lithium t-Butoxide: A New Route to Unsymmetrical 1,5- and 1,6-Diketones

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965
Hobbs, Peter D.; Upender, Velaparthi; Dawson, Marcia I.: Stereospecific Syntheses of Michellamines A and C

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968
Evans, P. Andrew; Nelson, Jade D.; Manangan, Thara: Preparation and Palladium Mediated Cross-Coupling Reactions of cis-2,3-Disubstituted 5-Halo-Dihydropyran-4-ones

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971
Göttlich, Richard; Yamakoshi, Koichi; Sasai, Hiroaki; Shibasaki, Masakatsu: A New and Selective Metal-Catalyzed Baeyer-Villiger Oxidation Procedure

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974
Arend, Michael; Risch, Nikolaus: A Simple and Highly Diastereoselective One-Pot Synthesis of Mannich-Bases

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977
Pietruszka, Jörg; Widenmeyer, Markus: Diastereoselective Synthesis of Cyclopropyl Boronic Esters

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980
Oishi, Tohru; Nagumo, Yoko; Hirama, Masahiro: Convergent Synthesis of a Trans-fused 6-7-6 Tricyclic Ether System Based on a Ring-closing Metathesis Reaction

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983
Sugai, Takeshi; Hamada, Keiji; Akeboshi, Tomohiro; Ikeda, Hajime; Ohta, Hiromichi: Biocatalyst-Mediated Efficient Preparation of Highly Enantiomerically Enriched (R)-5-Hexanolide

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986
Kvíala, Jaroslav; Plocar, Jakub; Vlasáková, Rena; Paleta, Oldich; Pelter, Andrew: 2-Fluoro-2-buten-4-olide, a New Fluorinated Synthon. Preparation; 1,2-, 1,4- and Tandem Additions

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989
Drew, Mark D.; Lawrence, Nicholas J.; Fontaine, David; Sehkri, Lakhdar; Bowles, Stephen A.; Watson, William: A Convenient Procedure for the Reduction of Esters, Carboxylic Acids, Ketones and Aldehydes using Tetrabutylammonium Fluoride (or Triton^® B) and Polymethylhydrosiloxane

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992
Crousse, Benoit; Alami, Mouâd; Linstrumelle, Gérard: Stereoselective Reduction of Conjugated Homopropargylic Alcohols to (E)-Homoallylic Alcohols by Sodium Bis(2-methoxyethoxy) Aluminium Hydride

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995
Khan, Faiz Ahmed; Czerwonka, Regina; Zimmer, Reinhold; Reissig, Hans-Ulrich: A Novel Sm(II)-Induced Route to Highly Substituted Benzannulated Cyclooctanol Derivatives

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998
Rigo, Benoît; Gautret, Philippe; Legrand, Anne; Hénichart, Jean-Pierre; Couturier, Daniel: Reaction of Trimethylsilyl Benzhydryl Ethers with Methyl N-(Trimethylsilyl)pyroglutamate: an Easy and Rapid N-Alkylation

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1001
Craig, Donald; Lawrence, Ronnie M.; Tapolczay, David J.: Stereoselective Synthesis of a Bicyclic Ketooxetane via a Thionium Ion-Mediated Cyclisation Reaction

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1004
Aurich, Hans Günter; Geiger, Michael; Sievers, Ulrich: Regio- and Diastereoselectivity in the Reaction Sequence from Secondary 3-Oxa-5-hexen-1-ylamines to Bicyclic Compounds via Nitrones

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1007
Fabian, Jeanne; October, Tessie; Cherestes, Alice; Engel, Robert: Polycations: Syntheses of Polyammonium Strings as Antibacterial Agents

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1010
Fürstner, Alois; Müller, Thomas: The First Synthesis of a 10-Membered Ring by Olefin Metathesis: Jasmine Ketolactone

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1013
Larsen, Scott D.: Novel Parham-type Cycloacylations of 1H-Pyrazole-1-alkanoic Acids

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