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Synlett 2000; 2000(6): 0815-0816
DOI: 10.1055/s-2000-6715
DOI: 10.1055/s-2000-6715
letter
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Facile "One-Pot" Preparation of Phosphonothiolformates. Useful Reagents for the Synthesis of Carbamoylphosphonates
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Publikationsverlauf
Publikationsdatum:
31. Dezember 2000 (online)
A versatile and mild "one-pot" reaction for the preparation of trialkyl phosphonothiolformates was accomplished by sequential reaction of phosgene solution with alkanethiols, and subsequent Arbuzov reaction with trialkyl phosphites.
phosphonic acids - phosphonothiolformates - carbamoylphosphonates - one pot reaction - Arbuzov reaction