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Synlett 2001; 2001(8): 1314-1316
DOI: 10.1055/s-2001-16040
DOI: 10.1055/s-2001-16040
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Montmorillonite K10 Clay-Microwave Assisted Isomerisation of Acetates of the Baylis-Hillman Adducts: A Facile Method of Stereoselective Synthesis of (E)-Trisubstituted Alkenes
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Publication History
Publication Date:
31 December 2001 (online)
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Montmorillonite K10-microwave assisted stereoselective isomerisation of acetates of the Baylis-Hillman adducts furnished (E)-trisubstituted alkenes in high yields. A comparative study of this reaction with Mont-K10, ion-exchanged clay (Fe3+-Mont-K10) and acid treated regional natural Kaolinite clay and the efficiency of these clays in this reaction is described.
montmorillonite K10 clay - microwave - stereoselective isomerisation - Baylis-Hillman reaction - E-alkenes - ion-exchanged clay - natural kaolinite clay