Download PDF
Synthesis 1995; 1995(3): 239-241
DOI: 10.1055/s-1995-4427
short paper
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.

A Practical Synthesis of Cycloalkylphosphonates from Trichloromethylphosphonates

Catherine Grandin, Noël Collignon* , Philippe Savignac
  • *Laboratoire des Composés Organophosphorés INSA-IRCOF, place E. Blondel, BP 08, F-76131 Mont-Saint-Aignan Cedex, France
Further Information

Publication History

Publication Date:
31 December 2000 (online)

  PDF Download  Permissions and Reprints All articles of this category

Cycloalkylphosphonates 5 with ring size varying from 4 to 6 were synthesized in good overall yields, in two steps from trichloromethylphosphonates and ω-dibromoalkanes, via the corresponding α-trimethylsilyl cycloalkylphosphonates 4.

Cycloalkylphosphonates 5 are prepared in two steps from trichloromethylphosphonates 1, via α-silylated cycloalkylphosphonates 4.