Taming SbH₃: A Simple and Safe Approach to Using Stibane in Synthesis on a Laboratory Scale

Abstract

Herein, we present a simple, inexpensive, and readily accessible apparatus for the safe and clean preparation, isolation, and conversion of stibane (SbH₃). In this setup, only typical standard glassware and fabric tubes are used. The pure stibane can be obtained in very good yields with very little expenditure of time.

Key words

antimony - stibane - inorganic chemistry - vacuum synthesis - gas induction

Publication History

Received: 02 February 2023

Accepted after revision: 20 March 2023

Article published online:
18 April 2023

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