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Synlett 1991; 1991(5): 319-320
DOI: 10.1055/s-1991-34730
DOI: 10.1055/s-1991-34730
letter
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.
A Facile Synthesis of (S,S)-(+)-and (R,R)-(-)-2,5-Bis(methoxymethy)pyrrolidine
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Publikationsverlauf
Publikationsdatum:
07. März 2002 (online)
![](https://www.thieme-connect.de/media/synlett/199105/lookinside/thumbnails/10.1055-s-1991-34730-1.jpg)
By the use of (S)-(-)-1-phenylethylamine as a chiral auxiliary as well as a nitrogen atom donor, (S,S)-(+)- and (R,R)-(-)-2,5- bis(methoxymethyl)pyrrolidine were synthesized from dimethyl meso-2,5-dibromoadipate through a short reaction sequence including stereoselective hydrolysis and chromatographic separation of intermediary diastereoisomers.