Synlett

Ausgabe 02 · Januar 2010

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165
Lu, Ping; Wang, Yanguang: Strategies for Heterocyclic Synthesis via Cascade Reactions Based on Ketenimines

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174
Marinetti, Angela; Voituriez, Arnaud: Enantioselective Phosphine Organocatalysis

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letter
195
Ibad, Muhammad Farooq; Abid, Obaid-Ur-Rahman; Nawaz, Muhammad; Adeel, Muhammad; Villinger, Alexander; Langer, Peter: Synthesis of 3,5-Diaryl-4-fluorophthalates by [4+2]-Cycloaddition and Subsequent Site-Selective Suzuki-Miyaura Reactions

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199
Khadem, Shahriar; Udachin, Konstantin A.; Arya, Prabhat: Solution- and Solid-Phase Synthesis of Tetrahydroquinoline-Based Polycyclics Having α,β-Unsaturated γ-Lactam and δ-Lactone Functionalities

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203
Okitsu, Takashi; Nakazawa, Daisuke; Kobayashi, Akihiro; Mizohata, Masahiro; In, Yasuko; Ishida, Toshimasa; Wada, Akimori: ipso-Iodocyclization of Ethoxyethyl Ethers to Alkynes at the ortho-Position: An Efficient Synthesis of Functionalized Spiro Compounds

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207
Bouziane, Asmae; Régnier, Thomas; Carreaux, François; Carboni, Bertrand; Bruneau, Christian; Renaud, Jean-Luc: A New Access to the 6,8-Dioxabicyclo[3.2.1]octane Ring System Using a Three-Component Reaction: Enantioselective Synthesis of (+)-iso-exo-Brevicomin

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211
Mangu, Naveenkumar; Spannenberg, Anke; Beller, Matthias; Tse, Man-Kin: Synthesis of Novel Annulated Hymenialdisine Analogues via Palladium-Catalyzed Cross-Coupling Reactions with Aryl Boronic Acids

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215
Brossard, Dominique; El Kihel, Laïla; Khalid, Mohamed; Rault, Sylvain: Synthesis of 6-Aryl-Substituted Cholesterol Derivatives from 3β-Acetoxy-6-iodocholest-5-ene and Arylboronic Acids Promoted by Palladium-Catalyzed Cross-Coupling

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219
Pelc, Matthew; Huang, Wei; Trujillo, John; Baldus, John; Turner, Steve; Kleine, Pete; Yang, Shengtian; Thorarensen, Atli: An Efficient and Regioselective Difluoromethylation of 3-Iodoindazole with Chlorodifluoromethane

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223
Jones, David M.; Dudley, Gregory B.: Synthesis of the C1-C15 Region of Palmerolide A Using Refined Claisen-Type Addition-Bond Cleavage Methodology

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227
Lu, Ping; Kuang, Jinqiang; Ma, Shengming: Carbon-Carbon Double-Bond Isomerization and Diels-Alder Reaction of Dimethyl 5-Methylene-4-isopropylidene-2-cycloheptene-1,1-dicarboxylate with Dienophiles

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231
Chen, Yan; Ju, Tong; Wang, Junwei; Yu, Wenquan; Du, Yunfei; Zhao, Kang: Concurrent α-Iodination and N-Arylation of Cyclic β-Enaminones

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235
Donghi, Monica; Pesci, Silvia; Summa, Vincenzo; Koch, Uwe; Spieser, Stephane; Gardelli, Cristina: Regioselective Synthesis of 7,8-Dihydropyrrolo[1,2-a]pyrimidin-4(6H)-ones and 7,8-Dihydropyrrolo[1,2-a]pyrimidin-2(6H)-ones

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240
Yadav, Lal Dhar S.; Singh, Santosh; Rai, Vijai K.: Carbonyl Umpolung Reactivity of Enals: NHC-Catalyzed Synthesis of Aldol Products via Epoxide Ring Opening

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247
Shen, Kaisheng; Livinghouse, Tom: A Stereocontrolled Synthesis of (±)-Ptilocaulin via a Rh(I)-Catalyzed Intramolecular [4+2] Cycloaddition

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250
Li, Bryan; Widlicka, Daniel W.; Buzon, Richard A.; Dou, Haijian; Granskog, Karl; Flanagan, Mark E.; Li, Bin; Liu, Fengwei; Liu, Wei; Magee, Thomas V.; Nguyen, Thuy-Trinh; Raggon, Jeffrey W.; Rainville, Joseph; Reilly, Usa Datta; Shen, Yue; Sun, Jianmin: A Scaleable Synthesis of 3-Hydroxy-1,5-naphthyridine-4-carbaldehyde

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253
Mihara, Masatoshi; Nakai, Takeo; Iwai, Toshiyuki; Ito, Takatoshi; Ohno, Toshinobu; Mizuno, Takumi: Solvent-Free Iron(III) Chloride Catalyzed O-, S-, and N-Acylation under Mild Conditions

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256
Sano, Shigeki; Tsumura, Takeshi; Tanimoto, Noriaki; Honjo, Takashi; Nakao, Michiyasu; Nagao, Yoshimitsu: Modified Cinchona Alkaloid-Zinc Complex Catalysts: Enantioselective Monoacetylation of Glycerol Derivatives with Acetic Anhydride

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261
Zhang, Chengyi; Gao, Xinqin; Zhang, Jianghua; Peng, Xiaojun: Fe/CuBr₂-Catalyzed Benzylation of Arenes and Thiophenes with Benzyl Alcohols

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266
Dong, Li-ting; Du, Quan-sheng; Lou, Chun-liang; Zhang, Jun-min; Lu, Rui-jiong; Yan, Ming: Asymmetric Synthesis of Nitrocyclopropanes Catalyzed by Chiral Primary Amines

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271
Vera-Ayoso, Yolanda; Borrachero, Pastora; Cabrera-Escribano, Francisca; Gómez-Guillén, Manuel; Caner, Joaquim; Farrás, Jaume: Easy Access to Configurationally Controlled C-Glycofuranoside-Based Building Blocks by Means of Formyl C-Glycofuranosides

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276
Hussain, Munawar; Zinad, Dhafer Saber; Salman, Ghazwan Ali; Sharif, Muhammad; Villinger, Alexander; Langer, Peter: Efficient Synthesis of Functionalized Anthraquinones by Domino Twofold Heck-6π-Electrocyclization Reactions of 2,3-Dibromonaphthoquinone

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cluster
281
He, Guangke; Xue, Can; Fu, Chunling; Ma, Shengming: An Efficient Synthesis of Allenyl Perfluoroalkyl Ketones from Mono-1,2-Addition-Elimination Reaction of Allenoates with R_fMgX

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286
Satoh, Tsuyoshi; Kasuya, Takashi; Miyagawa, Toshifumi; Nakaya, Nobuhito: Cyclobutylmagnesium Carbenoids: Generation from 1-Chlorocyclobutyl p-Tolyl Sulfoxides with Ethylmagnesium Chloride, Properties, and Some Synthetic Uses

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291
Tuulmets, Ants; Ploom, Anu; Panov, Dmitri; Järv, Jaak: Selectivity in the Grignard Reaction with Silanes

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294
Ackermann, Lutz; Wechsler, Cindy; Kapdi, Anant R.; Althammer, Andreas: Air-Stable Diaminophosphine Sulfides as Preligands for Nickel-Catalyzed Cross-Couplings of Unactivated Fluoro(hetero)arenes

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299
Cahiez, Gérard; Gager, Olivier; Buendia, Julien: New Insights into the Copper-Catalyzed Alkylation of Grignard and Organolithium Reagents

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304
Monzon, Gabriel; Knochel, Paul: Directed ortho- and meta-Magnesiation or Zincation of Polyfunctional Aryl Nonaflates

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309
Mitamura, Yukihiro; Someya, Hidenori; Yorimitsu, Hideki; Oshima, Koichiro: Silver-Catalyzed Diallylation and Dibenzylation of gem-Dibromoalkanes with Grignard Reagents

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313
Yoshikai, Naohiko; Matsumoto, Arimasa; Norinder, Jakob; Nakamura, Eiichi: Iron-Catalyzed Direct Arylation of Aryl Pyridines and Imines Using Oxygen as an Oxidant

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317
Ladjel, Chehla; Fuchs, Nicolas; Gremaud, Ludovic; Alexakis, Alexandre: Copper-Catalysed Kinetic Resolution of Cyclic Alkenyl Cyclopropane Malonates with Organoaluminium and Grignard Reagents

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321
Hatano, Manabu; Suzuki, Shinji; Ishihara, Kazuaki: Highly Chemoselective Stoichiometric Alkylation of Ketones with Grignard Reagent Derived Zinc(II) Ate Complexes

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325
Kobayashi, Yuichi; Tani, Yukio; Nakata, Kenya; Kaneko, Yuki: Allylic Substitution of 4-Cyclopentene-1,3-diol Monoacetate with Copper Reagents Derived from Functionalized Aryl Grignard Reagents

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329
Levin, Anat; Basheer, Ahmad; Marek, Ilan: Regiodivergent Carbometalation Reactions of Ynol Ether Derivatives

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spotlight
333
Liang, Huan: Triphenylcarbenium Tetrafluoroborate FREIER ZUGRIFF

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335
Goyal, Navneet: 1-Ethyl-3-(3-dimethylaminopropyl) Carbodiimide Hydrochloride (EDCI×HCl) FREIER ZUGRIFF

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addenda and errata
e2
Carbon-Carbon Double-Bond Isomerization and Diels-Alder Reaction of
Dimethyl 5-Methylene-4-isopropylidene-2-cycloheptene-1,1-dicarboxylate with Dienophiles FREIER ZUGRIFF

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