Synfacts

Issue 01 · January 2012

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SYNFORM ISSUE 2012/01 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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0001
Synthesis of MK-7655 FREE ACCESS

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0002
Synthesis of Gelsemoxonine

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0003
Synthesis of Pyripyropene A FREE ACCESS

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0004
Synthesis of a PDE IVb Inhibitor

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0005
Synthesis of Abamines

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0006
Synthesis of Vaniprevir (MK-7009)

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0007
Synthesis of (–)-Huperzine A

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0008
Formal Synthesis of (–)-Indatraline

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0009
Synthesis of Lonafarnib

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0010
Synthesis of Florfenicol

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0011
Synthesis of (+)-Yohimbine

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0012
Synthesis of (±)-Dragmacidin E

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0013
Synthesis of (±)-Hamayne

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0014
Synthesis of (–)-8-Demethoxyrunanine and (–)-Cepharatines A, C and D

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0015
Synthesis of (+)-Sertraline

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Synthesis of Heterocycles
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0017
Synthesis of Azabicyclo[3.1.1]heptane Derivatives from Cyclobutanones FREE ACCESS

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0018
Ni-Catalyzed Cycloaddition Approach to Fused Pyridine Derivatives

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0019
Phthalimide Synthesis via Oxidative Carbonylation of Benzamides

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0020
[3+2]-Dipolar Cycloaddition Route to 2H-Indazoles

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0021
Organocatalytic [3+2]-Cycloaddition Route to 1,2,3-Triazoles

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0022
Pd-Catalyzed Cross-Coupling–Lactonization Route to Dibenzopyranones

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0023
Concise Synthesis of Trifluoromethyl-Substituted Benzofuranols

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0024
Quinolines and Tetrahydroquinolines via Pd(0)-Catalyzed C–H Bond Functionalization

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0025
Intramolecular Heck-Type Synthesis of Piperideines and Pyridines

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0026
Synthesis of 3,4-Diaryl-3-pyrrolin-2-ones from Pyrrole Weinreb Amides

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0027
Pd-Catalyzed Synthesis of Furans from 1,3-Dicarbonyls and Propargylic Alcohols

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0028
Mitsunobu-Based Synthesis of Four-Membered Cyclic Oxaphosphetanes

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0029
Organocatalytic Enantioselective Synthesis of Functionalized Piperidines

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0030
One-Pot Synthesis of Benzo[b]furans from Phenols and Bromoalkynes

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0031
Stannous Chloride Mediated Synthesis of Spiroindolinone Quinazolines

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Synthesis of Materials and Unnatural Products
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0033
Polyenyne Cascade is Good as Gold

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0034
An Efficient Route to Tetrathia[7]helicenes

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0035
Taming 3,4-Dioxypyrroles

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0036
Steric Strain Driven BODIPY Functionalization

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0037
Switch the Light and the Carbenes!

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0038
Supramolecular Russian Dolls by Self-Assembly

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0039
Benzodipyrrolidone-Based Polymer: A New Donor–Acceptor Motif

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0040
Simple Synthesis of Buckybowls

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0041
Head-to-Tail-Type Oligothiophenes

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0042
A ’Smart’ Polymer Disassembles in Near Infrared Light

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0043
Coupling C,C-Diacetylenic Phosphaalkene this Way and that

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0044
Unsymmetrical 9,10-Dihydro-9,10-dibora-anthracenes

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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0045
Asymmetric Conjugate Addition Catalyzed by a Nickel–Diamine Complex

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0046
Gold-Catalyzed Diastereoselective Oxidative Cyclizations

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0047
Palladium-Catalyzed Asymmetric Allyl–Allyl Cross-Coupling FREE ACCESS

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0048
Cr(III)-Catalyzed AKR/ARO of Epoxides to β-Amino Alcohols

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0049
Asymmetric Monofluoromethylation by Co-operative Organo- and Lewis Acid Catalysis

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0050
Novel Carbohydrate-Derived Ligands for Asymmetric Transfer Hydrogenation

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0051
Asymmetric Approach to Chiral Pyrogluta-mates with a Quaternary Stereocenter

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0052
Rhodium-Catalyzed [2+2+2] Reaction of Ethynyl Ethers with Carbonyl Compounds

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0053
Iridium-Catalyzed Asymmetric Hydrogenation with Proline-Based P,O Ligands

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0054
Diastereoselective Cobalt-Catalyzed Multicomponent Couplings

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0055
Ni-Catalyzed Asymmetric α-Arylation and Heteroarylation of Ketones

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0056
Rhodium-Catalyzed Asymmetric Hydrogenation of Unsaturated Phosphonates

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0057
Advances in Nazarov Cyclizations through Control of [1,2]-Migrations

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0058
Palladium-Catalyzed Enantioselective Overman Rearrangement

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0059
Cationic Palladium Catalyzed Stereoselective Synthesis of Aminoindenes

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0060
Palladium-Catalyzed Stereoselective Transfer Hydrogenation of Alkynes

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0061
Cyclometalated Complex Library for Transfer Hydrogenation

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0062
Chiral Tetrahydroquinolines via an Aziridine Ring Opening/C–N Bond Formation Sequence

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0063
Scandium-Catalyzed Electrophilic Addition of α-Diazoesters with Ketones

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0064
New Cobalt Porphyrin Catalysts in Asymmetric Intramolecular Cyclopropanation

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0065
Pyrrolines via SnCl₄-Mediated [3+2] Cycloadditions of Cyclopropanes and Nitriles

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0066
Enantioselective and Regioselective Indium-Catalyzed Addition of Pyrroles to Isatins

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0067
Rhodium-Catalyzed 1:2 Coupling of Aldehydes with Allenes

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0068
Lewis Base Catalyzed Enantioselective Hypervinylogous Aldol Reactions

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0069
Trifluoromethylated Pyrrolidines via Cu-Mediated 1,3-Dipolar Cycloaddition

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0070
Catalyst-Controlled Gold-Catalyzed Carbocyclizations

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0071
Copper-Catalyzed Asymmetric Alkoxyamination

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0072
Asymmetric Synthesis of Amino Acids by Dehydrogenative Coupling

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0073
Regio- and Enantioselective Synthesis of Trifluoromethyl Allylic Amines

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Metal-Mediated Synthesis
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0075
Ag-Mediated C–H Trifluoromethylation of Aromatic Substrates

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0076
Direct Hiyama Coupling of Enaminones With Triethoxy(aryl)silanes

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0077
Boron–Ate Complexes as Chiral Nucleophiles for Asymmetric Synthesis FREE ACCESS

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0078
Cu-Catalyzed Enantioselective Addition of Alkynes to Isochroman Acetals

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0079
Selective Synthesis of Highly Substituted Isoquinolines

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0080
Total Synthesis of (+)-Erogorgiaene Using Lithiation–Borylation Methodology

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0081
Diastereoselective α-Trifluoromethylation of Carbonyl Compounds

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0082
Aldehydes in Bifunctional Titanocene-Catalyzed Propargylic C–X Activations

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0083
Scandium-Catalyzed Silylation of Aromatic C–H Bonds

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0084
Direct Synthesis of Alkynylstannanes from Tributyltin Methoxide and Alkynes

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0085
A New Method for the Synthesis of Difluoromethylated Aromatics

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0086
BiCl₃-Catalyzed Synthesis of Alkoxy- and Acetoxysilanes from Chlorosilanes

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0087
CoBr₂-Catalyzed Direct Allylation of Alkyl Halides

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0088
Chemo- and Regioselective Synthesis of Aluminoisoxazoles and Pyrazoles

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0089
Enantioselective Preparation and Chemo-selective Coupling of 1,1-Diboronyls

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Organo- and Biocatalysis
z91
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0091
NHC-Catalyzed Asymmetric Hydroacylation of Cyclopropenes

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0092
S_N2′–S_N2 Sequence of Morita–Baylis–Hillman Adducts

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0093
The Catalytic Asymmetric Fischer Indolization FREE ACCESS

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0094
Enantioselective Protonation via an Enamine Intermediate

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0095
Enantioselective Synthesis of α-Chiral 1,3-Azoles

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0096
α-Arylation of Enals via Aminocatalysis

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0097
Merging Organo- and Metal Catalysis

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0098
Asymmetric Allylic Trifluoromethylation of Morita–Baylis–Hillman Adducts

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0099
Stereoselective Addition of Azlactones to 3-Vinylindoles

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0100
Conjugate Addition Catalyzed by a Recyclable C₂-Symmetric Organocatalyst

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0101
Michael Addition/Nitronate-Olefin Cycloaddition/Fragmentation Sequence

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Polymer-Supported Synthesis
z103
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0103
One-Pot Tandem Reactions with a Bifunctional Solid Catalyst FREE ACCESS

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0104
Preparation of 3,4-Dihydroquinoxalin-2-amines Catalyzed by Amberlyst-15

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0105
Cu^II-MS4Å for Hydration of Nitriles into Amides

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0106
Hydrogenation of Unprotected Indoles with Platinum Catalysts

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0107
Hosomi–Sakurai Reaction with Silica Gel Supported Perchloric Acid

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0108
Catalytic Aerobic Oxidation of Alcohols with Pd@PMO-IL

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0109
Aerobic Oxidation of Alcohols with Au/MgCr-Hydrotalcite

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0110
Synthesis of Quinolines from ArNO₂ and Alcohols with Ir/TiO₂-NCs

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0111
Intermolecular Coupling of Alkynes with Acrylates Using Ru/CeO₂

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0112
Preparation of Benzimidazoles via Oxidation of Tertiary Amines

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0113
Solvent-Free Hydrogenation and Suzuki–Miyaura Coupling Using Pd/C

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0114
Hydrolysis of VX Using Solid-Supported Ammonium Fluorides

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0115
Friedel–Crafts Addition of Indoles Using Graphite Oxide

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0116
Synthesis of Hydroxy-1,2,3-Triazoles with Cu Nanoparticles on Activated Carbon in Water

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