Synfacts

Issue 03 · March 2012

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SYNFORM ISSUE 2012/03 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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0233
Synthesis of (+)-Sertraline FREE ACCESS

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0234
Synthesis of Hyperpapuanone

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Synthesis of (+)-Saxitoxin

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Synthesis of (±)-Peribysin E

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0237
Synthesis of Tulearin C

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0238
Synthesis of β-Adrenergic Blockers

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0239
Synthesis of (S)-Naproxen

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0240
Synthesis of (–)-Benzolactam-V8

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0241
Synthesis of Brevianamide E

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0242
Synthesis of (–)-Arabilin

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0243
Synthesis of (+)-Taxadiene

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0244
Formal Synthesis of Beraprost

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0245
Synthesis of Ulimorelin

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Synthesis of Heterocycles
z247
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0247
One-Pot Heteroannulative Synthesis of α-Carbolines from 2-Aminoindoles

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0248
Diastereoselective Narasaka–Heck Route to Bicyclic N-Heterocycles

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0249
Organocatalytic Enantioselective Friedel–Crafts Approach to 2,3-Dihydrobenzofurans

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0250
Pd-Catalyzed Multicomponent Synthesis of 4-Aminophthalazin-1(2H)-ones

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0251
Pd-Catalyzed Synthesis of Dibenzoazepines from 2-Bromoanilines

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0252
Multicomponent Synthesis of Benzo[a]pyrano[2,3-c]phenazines

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0253
Regiospecific Synthesis of Polysubstituted Pyridines

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0254
Regioselective Arylation of Pyridine N-Oxides via Silver-Catalyzed C–H Activation

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0255
Concise Synthesis of Tetrahydro-5H-indolo[3,2-c]quinolines

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0256
Synthesis of Nitrated Triazoles as Potentially New Explosives

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0257
Oxidative Expansion of Oxiranes and Oxetanes via Copper Catalysis

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0258
Azetidines, Pyrrolidines, and Indolines via C(sp³)–H and C(sp²)–H Bond Amination

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0259
Tetrahydro-1,4-benzodiazepin-2-ones from Ugi MCR Intermediates FREE ACCESS

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0260
Fused Pyridazino[4,5-b]oxazepine-diones via Smiles Rearrangement

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0261
Copper-Catalyzed Synthesis of 2H-Isoindole-1-Carboxylates

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Synthesis of Materials and Unnatural Products
z263
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0263
peri-Cyclization of Ethynylene Naphthalene Oligomers

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0264
Bis-Bispidine Tetraazamacrocycles with Handles

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0265
‘Double Rainbow (All the Way)’ to Rhodamines

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0266
Luminescent Bora-Cyclophanes

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0267
New Near-IR Fluorophores

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0268
An Unusual Chain-Growth Polymerization of Naphthalene Diimide

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0269
One-Pot Syntheses of Tetrathienoacenes

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0270
Side-Dimerization of Pentacene

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0271
Three-Leaf Clover-Shaped Nanographenes

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0272
n-Type to the Core

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0273
Shape-Persistent 3D Molecular Cage

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0274
Highly Refractive Transparent Polymers by Design

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0275
A New Path Toward Substituted Phenanthrenes

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z277
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0277
Rh-Catalyzed Enantioselective Coupling of Allenes with Carboxylic Acids

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0278
Enhanced Enantioselectivity by Chiral Alcohol Additives in Asymmetric Hydrogenation

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0279
Asymmetric Synthesis of Stable Oxetenes via [2+2] Cycloaddition FREE ACCESS

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0280
Asymmetric Iridium-Catalyzed Hydrogenation of Birch Products

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0281
Zinc-Catalyzed Asymmetric α-Alkylallylation of Aldehydes FREE ACCESS

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0282
Kinetic Resolution via Palladium-Catalyzed Asymmetric Allylation

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0283
Enantioselective Diels–Alder Reactions Using Chiral Supramolecular Catalysts

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0284
Enantioselective Diboration of 1,3-Dienes and Stereoselective Allyation

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0285
Asymmetric Ring Opening of Oxabicyclic Alkenes with Organolithium Reagents

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0286
Palladium-Catalyzed Enantioselective Addition of Benzyl Nitriles to Imines

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0287
Cu(I)-Catalyzed 1,2-Additions to α-Methyl-Substituted α,β-Unsaturated Ketones

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0288
Enantioselective Synthesis of Chiral 1,3-Diaminopropanols

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0289
Pd(II)-Catalyzed Asymmetric Hydrophosphination of Dienones

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0290
Asymmetric Allylation and Crotylation of β,γ-Unsaturated Aldehydes

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0291
Palladium-Catalyzed Diastereoselective Synthesis of Chromans

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0292
Palladium-Catalyzed Asymmetric Hydrocarbonation of Oxyallenes

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0293
Copper-Catalyzed Enantioselective Hydro-silylation of Dialkyl and Aryl-Alkyl Ketones

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0294
Rhodium(II)-Catalyzed Asymmetric Cycloaddition of Carbonyl Ylides with Indoles

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0295
Asymmetric Synthesis of Cyclopropanes Bearing Two Chiral Quaternary Centers

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0296
Synthesis of Hydroindolones by [5+1] Annulation

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0297
Zinc(II)-Catalyzed Enantioselective Synthesis of α-Aminophosphonates

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0298
Palladium-Catalyzed Asymmetric Diastereodivergent Deracemization

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0299
Palladium-Catalyzed Stereoselective Double-Bond Migration

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0300
Cu-Catalyzed Asymmetric Conjugate Addition of Glycine Derivatives

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0301
Rh(I)-Catalyzed Asymmetric Hydrogenation of α- and β-Enamido Phosphonates

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0302
Nickel-Catalyzed Diastereoselective [3+2] Cycloaddition

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0303
Zn-Catalyzed 1,4-Additions of Dialkyl Phosphine Oxides to α,β-Carbonyls

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0304
Catalytic Asymmetric Addition of Aryl Bromides to Aldehydes

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0305
Palladium-Catalyzed Cross-Coupling of Cyclopropanes with Organoboron Reagents

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Metal-Mediated Synthesis
z307
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0307
Tandem One-Pot Synthesis of Tertiary Alcohols

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0308
Stereoselective Vinylation of Aryl N-(2-Pyridylsulfonyl) Aldimines

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0309
Tandem One-Pot Synthesis of Polysubstituted Pyridines FREE ACCESS

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0310
Diquinanes and Hydrindanes by Michael Aldol and Baylis–Hillman Reactions

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0311
Synthesis of Amides via AlMe₃-Promoted Coupling of Acids and Amines

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0312
Regioselective Hydrosilylation of Alkynes Using a Dimethylvinylsilyl Group

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0313
Tin-Mediated Fragmentation to Yield Medium-Sized Cyclic 2-Alkynones

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0314
Synthesis of Cyclopentenones by Pseudo-Pauson–Khand Cyclization

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0315
Selective Inversion and Retention in Stereospecific Suzuki–Miyaura Coupling

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0316
Selective Transformations of Carbonyl Groups in the Presence of Aldehydes

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0317
Cu-Mediated Directed ortho C–H Nitration of (Hetero)arenes

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0318
Aliphatic α,α-Difluoro-β³-Amino Esters via Sonocatalyzed Reformatsky Reaction

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0319
Pd-Catalyzed Trifluoromethylation of Vinyl Sulfonates

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0320
Coupling of Aryl Grignard Reagents with Aryl Halides through S_RN1 Pathway

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0321
Reversed-Polarity Synthesis of Diaryl Ketones

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Organo- and Biocatalysis
z323
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0323
One-Pot Strategy to Isochromene Pyrimidinedione Derivatives

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0324
Brønsted Acid Catalyzed Asymmetric Propargylation of Aldehydes

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0325
Asymmetric Counteranion Directed Phase-Transfer Catalysis FREE ACCESS

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0326
Hydroxylamine-Based ‘Inorganocatalysis’ of Transamidations

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0327
Combining Mechanochemical Racemization with Enzymatic Resolution

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0328
Enantioselectivity Switch Induced by an Achiral Acid

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0329
Organocatalytic Route to 3-Substituted 3-Hydroxyoxindoles

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0330
Proline-Based Tautomerase Catalyzed Michael Addition

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0331
Enantioselective [3+2] Cyclizations Catalyzed by a Dipeptide-Based Phosphine

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0332
Synthesis of 3-Difluoroalkyl 3-Hydroxy-oxindoles

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0333
Synthesis of Axially Chiral Anilides by Phase-Transfer-Catalyzed N-Alkylations

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Polymer-Supported Synthesis
z335
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0335
N-Methylated Nitrogen-Doped Mesoporous Silica as a Solid-Base Catalyst

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0336
TiO₂–SO₄^2–Catalyst for the Preparation of Quinoxalines and Dipyridophenazines

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0337
A Flow System for Enantioselective Carbonyl Ylide Cycloaddition FREE ACCESS

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0338
Suzuki–Miyaura Coupling of ArN₂BF₄ with Supported Palladium Nanoparticles

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0339
Hydroxylation of Aryl Iodides with CsOH Using Mesoporous Silica-Supported CuO

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0340
Cyanosilylation of Aldehydes with Microporous Aluminoborates

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0341
Preparation of Fe–MoO_x/Polyaniline Nanorods as Epoxydation Catalysts

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0342
An MCM-41-Anchored Sulfonic Acid Catalyst for Strecker Reaction

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0343
Synthesis of Dithiocarbamates with Nanocrystalline MgO

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0344
Intramolecular Friedel–Crafts Reaction of Azlactones Using H₃PW₁₂O₄₀/Al₂O₃

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0345
Carbonylative Synthesis of N-Substituted Phthalimides Using Pd/C

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0346
Suzuki–Miyaura Coupling with BIO-Immobilized Palladium Catalyst

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0347
Oxidation of Alkenes, Amines, Silanes and Sulfides Using W–Zn/SnO₂

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Addenda and Errata
0348
Bis-Phosphoric Acid: Two is Better than One

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