Synlett

Issue 03 · February 2004

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Rawat, Diwan S.; Zaleski, Jeffrey M.: Geometric and Electronic Control of Thermal Bergman Cyclization

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422
Berndt, Mathias; Gross, Steffen; Hölemann, Alexandra; Reissig, Hans-Ulrich: New Samarium Diiodide-Induced Ketyl Couplings - From Analogous Reactions to Serendipitously Discovered Processes

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439
Ulrich, Gilles; Ziessel, Raymond: Highly Luminescent Probes from Terpyridine, Phenanthroline, and Pyrromethene·BF₂ Auxiliaries

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445
Liu, Yongjun; Xu, Xiaoliang; Zhang, Yongmin: Direct Formation of Benzoins from Diarylmethanones via a Rearrangement Reaction Promoted by Samarium Metal in DMF

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449
Panda, Kausik; Siddiqui, Iffat; Mahata, Pranab K.; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar: Heteroannulation of 3-Bis(methylthio)acrolein with Aromatic Amines -
A Convenient Highly Regioselective Synthesis of 2-(Methylthio)quinolines and their Benzo/Hetero Fused Analogs - A Modified Skraup Quinoline Synthesis

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453
Oliver, Morag; Jorgensen, Michael R.; Miller, Andrew D.: Solid-Phase Assisted N-1 Functionalization of Azamacrocycles

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457
Higashibayashi, Shuhei; Tohmiya, Hiraku; Mori, Tomonori; Hashimoto, Kimiko; Nakata, Masaya: Synthesis of Sulfinimines by Direct Condensation of Sulfinamides with Aldehydes Using Cs₂CO₃ as an Activating and Dehydrating Reagent

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461
Braddock, D. Christopher; Cansell, Gemma; Hermitage, Stephen A.: (Diacetoxyiodo)benzene-Lithium Bromide as a Convenient Electrophilic Br⁺ Source

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465
Zhu, Chengjian; Yang, Minghua; Sun, Jiangtao; Zhu, Yuhua; Pan, Yi: The Synthesis of New C₂-Symmetric Chiral 1,4-Diamino Motif and Application in Catalytic Asymmetric Alkynylation of meso-Epoxides

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469
Wang, Xiang-Zhu; Burke Jr, Terrence R.: Enantioselective Synthesis of Metathesis-Derived Ureapeptoid Macrocycles

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473
Olsen, Christian A.; Witt, Matthias; Jaroszewski, Jerzy W.; Franzyk, Henrik: Diols as Building Blocks in Solid-Phase Synthesis of Polyamine Toxins by Fukuyama-Mitsunobu Alkylation

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477
Miyazaki, Tohru; Han-ya, Yuki; Tokuyama, Hidetoshi; Fukuyama, Tohru: New Odorless Protocols for the Synthesis of Aldehydes and Ketones from Thiol Esters

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481
Nagao, Yoshimitsu; Tanaka, Satoru; Hayashi, Kazuhiko; Sano, Shigeki; Shiro, Motoo: New Synthetic Methods for Seven- and Eight-Membered Cyclic Ethers Based on the Ring-Expansion Reactions of Hydroxy or Lithioxy Methoxyallenylisochroman Derivatives

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485
Xu, Chengfu; Zhang, Yonghui; Yuan, Chengye: A Chemoenzymatic Approach to Optically Active 5-Hydroxy-3-oxo-carboxylates

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489
Suh, Man-Jin; Kim, Sang Woo; Beak, Seong In; Ha, Hyun-Joon; Lee, Won Koo: Highly Stereoselective Addition of Organomagnesium Reagents to Aziridinyl-2-carboxaldimine: Preparation of Enantiopure 2-Aminomethylaziridines and 4,5-Disubstituted Imidazolidin-2-ones

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493
Sureshan, Kana M.; Watanabe, Yutaka: Simple and Efficient Routes to Optically Active chiro- and allo-Inositol Derivatives from myo-Inositol

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497
Amaya, Toru; Tanaka, Hiroshi; Takahashi, Takashi: Combinatorial Synthesis of Carbohydrate Cluster on Tree-Type Linker with Orthogonally Cleavable Parts

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503
Amaya, Toru; Tanaka, Hiroshi; Takahashi, Takashi: Solid-Phase Synthesis of Carbohydrate Cluster on Tree-Type Linker with Three Types of Orthogonally Cleavable Part

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508
Ohno, Hiroshi; Tanaka, Hiroshi; Takahashi, Takashi: Solid-Phase Synthesis of N-Alkylated Naltrindoles Using a 3-Nitrobenzyl Safety-Catch Linker

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512
Chanteau, Frédéric; Plantier-Royon, Richard; Portella, Charles: Synthesis of Fluorinated Homo-C-Nucleoside Analogues from New Carbohydrate-Derived Acylsilanes

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517
Ma, Zhen; Liu, Shi-Xiong: Unexpected Dimerization of a N₅O₃ Cryptand in Aqueous Solution after Being Protonated by Hydrochloric Acid

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522
Chandrasekhar, S.; Shyamsunder, T.; Chandrashekar, G.; Narsihmulu, Ch.: Hydrogenation and Hydrogenolysis with Pd/C in Poly(Ethylene Glycol) (PEG): A Practical and Recyclable Medium

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525
Kantam, M. Lakshmi; Neeraja, V.; Kavita, B.; Haritha, Y.: Cu(acac)₂ Immobilized in Ionic Liquids: A Novel and Recyclable Catalytic System for Aziridination of Olefins Using PhI=NTs as Nitrene Donor

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528
Knölker, Hans-Joachim; Krahl, Micha P.: Transition Metal Complexes in Organic Synthesis, Part 71: First Total Synthesis of Furoclausine-A

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531
Paul, Satya; Nanda, Puja; Gupta, Rajive: Solvent-Free Benzylic Oxidations Using Urea-Hydrogen Peroxide Complex (UHP) under Microwave Irradiation

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534
Lu, Jun; Ji, Shun-Jun; Qian, Rong; Chen, Jian-Ping; Liu, Yu; Loh, Teck-Peng: InCl₃-Promoted Allylation of Aldehydes in Ionic Liquid: Scope and Enantioselectivity Studies

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537
Tu, Shujiang; Fang, Fang; Zhu, Songlei; Li, Tuanjie; Zhang, Xiaojing; Zhuang, Qiya: A New Biginelli Reaction Procedure Using Potassium Hydrogen Sulfate as the Promoter for an Efficient Synthesis of 3,4-Dihydropyrimidin-2(1H)-one

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540
Miyabe, Hideto; Asada, Ryuta; Yoshida, Kazumasa; Takemoto, Yoshiji: Free Radical-Mediated Tandem Reaction of Dehydroamino Acid Derivative with π-Allyl Palladium Complex: Synthesis of α,α-Disubstituted Amino Acids

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543
Patterson, Brian; Rychnovsky, Scott D.: Mukaiyama Aldol-Prins Cyclizations with Ketones

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546
Arasaki, Hideki; Iwata, Masashi; Nishimura, Daisuke; Itoh, Akichika; Masaki, Yukio: Stereospecific Construction of Chiral Quaternary α-Oxygenated Aldehydes from Chiral Secondary Alcohol Derivatives

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549
Attanasi, Orazio A.; De Crescentini, Lucia; Favi, Gianfranco; Filippone, Paolino; Mantellini, Fabio; Santeusanio, Stefania: Expeditious Synthesis of 1,2-Diaminoimidazoles under Solvent-Free Conditions

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552
Chen, Jiang-Min; Huang, Xian: The First Example of Polymer-supported Alkenyl Iodonium Salts: Efficient Synthesis of β-Functional Enamines

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555
Ding, Rui; Zhang, Hai Bo; Chen, Yong Jun; Liu, Li; Wang, Dong; Li, Chao Jun: In(OTf)₃-Catalyzed Friedel-Crafts Reaction of Aromatic Compounds with Methyl Trifluoropyruvate in Water

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558
Cobb, Alexander J. A.; Shaw, David M.; Ley, Steven V.: 5-Pyrrolidin-2-yltetrazole: A New, Catalytic, More Soluble Alternative to Proline in an Organocatalytic Asymmetric Mannich-type Reaction

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561
Wang, Chun-Yan; Su, Hua; Yang, De-Yu: Regio- and Stereoselective Dimerization of Terminal Alkynes to Enynes in InCl₃-NaBH₄-MeCN System

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new tools in synthesis
564
Lellouche, Jean-Paul; Kotlyar, Vadim: Vilsmeier-Haack Reagents. Novel Electrophiles for the One-Step Formylation of O-Silylated Ethers to O-Formates

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spotlight
572
O’Mahony, Gavin: Triethylborane (Et₃B) FREE ACCESS

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574
Ghosh, Nandita: DBU (1,8-diazabicyclo[5.4.0]undec-7-ene) - A Nucleophillic Base FREE ACCESS

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errata
576
Sonavane, Sachin U.; Jayaram, Radha V.: Selective Reduction of C=O in α,β-Unsaturated Carbonyls through Catalytic Hydrogen Transfer Reaction over Mixed Metal Oxides FREE ACCESS

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576
Sarkar, Sandipan: Trifluoromethanesulfonic (triflic) Anhydride FREE ACCESS

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