DOI: 10.1055/s-00000083

Synlett

Issue 02 · Volume 24 · January 2013 DOI: 10.1055/s-003-24354

synpacts

139
Gao, Lu; Zhang, Yuebao; Song, Zhenlei: Exploration of Versatile Geminal Bis(silane) Chemistry
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145
Wang, Chengming; Huang, Yong: Expanding Structural Diversity; Removable and Manipulable Directing Groups for C–H Activation
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account

150
Bornscheuer, Uwe T.: From Commercial Enzymes to Biocatalysts Designed by Protein Engineering
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letter

157
Guignard, Raphaël F.: A Concise Total Synthesis of the Purported Structure of Flossonol
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Supporting Information
161
Yavari, Issa; Nematpour, Manijeh; Sodagar, Esmat: Copper-Catalyzed Tandem Synthesis of Highly Functionalized Bisamidines
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165
Yavari, Issa; Nematpour, Manijeh: Copper-Catalyzed Tandem Synthesis of Tetrasubstituted Pyrimidines from Alkynes, Sulfonyl Azides, Trichloroacetonitrile, and Tetramethylguanidine
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169
Garrido, Narciso M.; Nieto, Carlos T.; Díez, David: Enantioselective Synthesis of a (1R,5R,9R)-2-Azabicyclo[3.3.1]nonane-9-carboxylic Acid with an Embedded Morphan Motif: A Multipurpose Product
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173
Ravi, Makthala; Anand, Devireddy; Maurya, Ranjani; Chauhan, Parul; Naikade, Niraj K.; Shukla, Sanjeev K.; Yadav, Prem P.: Synthesis of 1,2,4-Trioxepanes and 1,2,4-Trioxanes via H2O2-Mediated Reaction of Tertiary Carbinols
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Supporting Information
177
Niermann, André; Grössel, Janine E.; Reissig, Hans-Ulrich: New Thiochromans via Reductive Cyclization of Thiophenol Derivatives
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181
Rodríguez-Solla, Humberto; Concellón, Carmen; Alvaredo, Noemí; Llavona, Ricardo; García-Granda, Santiago; Díaz, M. Rosario; Soengas, Raquel G.: Stereoselective Synthesis of Carbohydrate-Derived N-Sulfonyl Aziridines
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Supporting Information
185
Duffy, Liam J.; Garcia-Torres, Jason; Jones, Raymond C. F.; Elsegood, Mark R. J.; Allin, Steven M.: Application of a Dual Fries–Claisen Protocol to Access Pyranonaphthoquinone Natural Products
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189
Chen, Cheng-yi; Weisel, Mark: Concise Asymmetric Synthesis of (+)-Conocarpan and Obtusafuran
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193
Jiang, Tao; Huynh, Khoi; Livinghouse, Tom: Substrate Structural Effects in Yttrium(III)-Catalyzed Hydroamination/Cyclizations of 1,2-Disubstituted and 1,1,2-Trisubstituted Aminoalkenes ­Terminated by 2-(Phenyl) and 2-(2-Heteroarenyl) Groups
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Supporting Information
197
Kuroboshi, Manabu; Yamamoto, Takashi; Tanaka, Hideo: Amphiphilic Viologen: Electrochemical Generation of Organic Reductant and Pd-Catalyzed Reductive Coupling of Aryl Halides in Water
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201
Choi, Lai-Sheung; Chow, Hak-Fun: Versatile Synthesis of Amphiphilic Oligo(Aliphatic-Glycerol) Layer-Block Dendrons with Different Hydrophilic-Lipophilic Balance Values
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Supporting Information
207
Osawa, Ayumi; Mera, Akane; Namba, Kosuke; Tanino, Keiji: Transformations of 1-(Oxiranylmethyl)-1,2,3-triazoles into 2-(Oxiranyl­methyl)-1,2,3-triazoles and Alkanenitriles
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211
He, Hua-Feng; Wang, Kai; Xing, Bo; Sheng, Guorong; Ma, Tingxuan; Bao, Weiliang: Formation of C–O Bond via Cross-Dehydrogenative Coupling between Isochroman and Oxime under Metal-Free Oxidation Conditions
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Supporting Information
215
Jiang, Zhihui; Ni, Tingjunhong; Wei, Changqing; Tian, Shujuan; Li, Yan; Dai, Li; Liu, Hong; Zhang, Dazhi: Selectfluor-Promoted Direct Fluorination at the 4- or 5-Position of Imidazole Derivatives
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Supporting Information
219
Pradhan, Tapan Kumar; Lin, Chun Cheng; Mong, Kwok Kong Tony: Formal Synthesis of 3-Deoxy-d-manno-Octulosonic Acid (KDO) and 3-Deoxy-d-arabino-2-heptulosonic Acid (DAH)
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Supporting Information
223
Samimi, Heshmat A.; Mohammadi, Somaye: A New Approach to Ring Expansion of Keto Aziridines to 2,5-Diaryloxazoles
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Supporting Information
226
Pazynina, Galina; Tyrtysh, Tatiana; Nasonov, Vitaly; Belyanchikov, Ivan; Paramonov, Alexander; Malysheva, Nelly; Zinin, Alexander; Kononov, Leonid; Bovin, Nicolai: Divergent Strategy for the Synthesis of α2-3-Linked Sialo-oligosaccharide Libraries Using a Neu5TFA-(α2-3)-Gal Building Block
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Supporting Information
231
Schou, Simon Stubbe; Parker, Christian Richard; Lincke, Kasper; Jennum, Karsten; Vibenholt, Johan; Kadziola, Anders; Nielsen, Mogens Brøndsted: On the Phosphite-Mediated Synthesis of Dithiafulvenes and π-Extended Tetrathiafulvalenes
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Supporting Information
236
Sobhani, Sara; Honarmand, Moones: A Simple and Efficient Method for One-Pot, Three-Component Synthesis of Terminal Vinylphosphonates Using a Task-Specific Ionic Liquid
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Supporting Information
241
Pan, Li; Chen, Ruijiao; Ni, Dongshun; Xia, Liang; Chen, Xiaochuan: An Approach to the Synthesis of Enantiopure Tetrahydroisoquinoline via a Key Asymmetric Ugi Reaction
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Supporting Information
246
Mahmood, Javeed; Kim, Dongwook; Jeon, In-Yup; Lah, Myoung Soo; Baek, Jong-Beom: Scalable Synthesis of Pure and Stable Hexaaminobenzene Trihydrochloride
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Supporting Information
249
Franconetti, Antonio; Borrachero, Pastora; Gómez-Guillén, Manuel; Cabrera-Escribano, Francisca: Toward Fluorinated Aminoglycosides: Structural Studies of Phenylhydrazine Condensation with Carbohydrate Derivatives
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254
Hajipour, Abdol Reza; Azizi, Ghobad: The [RPPh3]2[Pd2X6] as a Catalyst Precursor for the Heck Cross-Coupling Reaction by in situ Formation of Stabilized Pd(0) Nanoparticles
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Supporting Information
259
Gille, Marie; Viertel, Andreas; Weidner, Steffen; Hecht, Stefan: Modular Synthesis of Monomers for On-Surface Polymerization to Graphene Architectures
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Supporting Information

spotlight

264
Faria, Jéssica Venância: Ethoxymethylenemalononitrile
266
Zhang, Jichao: 2-Cyanoethyl N,N,N′,N′-Tetraisopropylphosphorodiamidite

erratum

268
Palmieri, Alessandro; Gabrielli, Serena; Ballini, Roberto: An Improved, Fully Heterogeneous, Diastereoselective Synthesis of (Z)-α-Bromonitroalkenes