Synfacts

Issue 06 · June 2013

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SYNFORM ISSUE 2013/06 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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0577
Synthesis of an Adenosine A_2A Receptor Antagonist

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0578
Synthesis of 1,1-Diphenylpropyl-1-amines via Hydroaminomethylation

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0579
Synthesis of Tatanans A–C and Their Glucokinase-Activating Properties FREE ACCESS

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0580
Synthesis of (+)-Plectosphaeroic Acid B

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0581
Synthesis of BI 201302 FREE ACCESS

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0582
Total Synthesis of Spirocurcasone

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0583
Total Synthesis of Cyanolide A

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0584
Synthesis of GPI 16539

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0585
Synthesis of Atorvastatin

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0586
Synthesis of Spiropiperidine BACE-1 Inhibitors

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0587
Syntheses of Taiwaniaquinone F and Taiwaniaquinol A

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0588
Total Synthesis (+)-Roseophilin

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0589
Total Synthesis of (±)-Leuconolam

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0590
Asymmetric Synthesis of cis-2,5-Disubstituted Pyrrolidines

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0591
Synthesis of a Sodium–Hydrogen Exchange Type 1 Inhibitor

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Synthesis of Heterocycles
z593
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0593
Synthesis of Pyrazolo[1,5-a]pyrimidines

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0594
Synthesis of Indolizinones via Sequential Ritter and Pictet–Spengler Reactions

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0595
Functionalized γ-Lactams via Dess–Martin Periodinane Oxidation of Pyrroles

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0596
Intramolecular Cyclization Route to Disubstituted 4-Selenyl Isoxazoles

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0597
Palladium-Catalyzed Oxidative Isocyanide Insertion for Heterocyclic Synthesis

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0598
Synthesis of Substituted 1,2,4-Triazoles from Formamidrazones and Isocyanides

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0599
Iridium-Catalyzed Synthesis of Pyrroles from Secondary Alcohols and β-Amino Alcohols

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0600
Expedient Access to Biologically Relevant Furan-Based Scaffolds

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0601
Scalable Approach to 4-Aminopyrimidines

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0602
A Three-Component Copper-Catalyzed Synthesis of Bicyclic Isoxazolidines

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0603
Synthesis of Trisubstituted Imidazoles via Oxidative Diamination of Alkynes

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0604
A Copper-Catalyzed [3+2]-Cycloaddition Route to Substituted Imidazoles

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0605
C–H Activation Route to Phthalazinones from N′-Methylenebenzohydrazides

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0606
2-Aryl-3-fluoro-5-silylthiophenes via a [2,3]-Sigmatropic Rearrangement

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Synthesis of Materials and Unnatural Products
z607
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0607
Large, Yet Soluble, Polycyclic Aromatics

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0608
exo-Olefin-Terminated Polyisobutylene via Ether Quenching

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0609
A One-Step, Two-Component, Triple Domino Process to Tetrasubstituted Alkenes

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0610
Cyclic Oligofluoranthene in One Step

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0611
A Novel Electron-Accepting Scaffold for Organic Electronics

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0612
Synthesis of Borylated Dibenzoborepin via Skeletal Rearrangement

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0613
Low Band Gap Conjugated Polymer Synthesis

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0614
Solvent-Free Synthesis of Pyrrolophenanthrolines via Multicomponent Reactions

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0615
Synthesis of Hexa(furan-2-yl)benzenes and Their π-Extended Derivatives

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0616
Cyclodimerization Leads to a Fluorene-Containing Aromatic Framework

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0617
Twisted Polycyclic Arenes by Intramolecular Scholl Reactions

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0618
Heterotriangulene Macrocycles toward Honeycomb Networks

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z619
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0619
Calcium-Catalyzed Cyclopropanation

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0620
Cooperative Oxovanadium–Lipase System for Dynamic Kinetic Resolution

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0621
Asymmetric Iron–Brønsted Acid Catalyzed Hydrogenation

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0622
Scandium-Catalyzed Asymmetric Mannich Reaction

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0623
Nickel-Catalyzed 1,3-Dipolar Cycloadditions to Pyrazolones

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0624
Copper-Catalyzed Friedel–Crafts Alkylation–N-Hemiacetalization

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0625
Redox-Independent Ruthenium-Catalyzed [4+2] Cycloaddition

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0626
Asymmetric Iron-Catalyzed N₃-Transfer Using Azoiodinane

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0627
Chiral Oxazolidine Diene Ligands for Asymmetric Conjugate Additions

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0628
Ruthenium-Catalyzed Intramolecular Silylvinylation of Internal Alkynes

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0629
Rhodium-Catalyzed Asymmetric Domino Transformation

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0630
Rhodium-Catalyzed Asymmetric Synthesis of Oxazolidinone Scaffolds

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0631
Y(III)–Arylamine System for Cooperative Enamine–Lewis Acid Asymmetric Catalysis

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0632
Asymmetric Epoxidation of Allylic Alcohols by Chiral Dihydroperoxides

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0633
Asymmetric Addition Reaction of Organoboronic Acids to Aldehydes

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0634
Rhodium-Catalyzed Asymmetric [2+2+2] Cycloaddition of Diynes

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0635
Copper(II)-Catalyzed Asymmetric Henry Reaction

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0636
Rhodium-Catalyzed Enantioselective Alkynylation of Trifluoropyruvates

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0637
Copper-Catalyzed Regio- and Enantioselective Hydroboration

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0638
Hafnium(IV)-Catalyzed Epoxidation of Tertiary Olefinic Alcohols

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0639
Copper-Catalyzed Conjugate Addition to α,β-Unsaturated Lactams

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0640
Redox-Neutral [4+2]-Annulation Reaction via Rhenium–Magnesium Catalysis

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0641
Gold-Catalyzed Hetero-Diels–Alder Reaction of Diazenes

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0642
Copper(I)-Catalyzed Asymmetric Allylic Oxidation of Cycloolefins

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0643
Enantioselective Nitro-Michael Addition to (E)-2-Azachalcones

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0644
Synthesis of Brominated Enamines via Palladium-Catalyzed Aminohalogenation

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0645
Copper-Catalyzed Vinylogous Mukaiyama–Michael Addition Reactions

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0646
Nickel-Catalyzed Enantioselective Synthesis of Diarylalkanes and Triarylmethanes

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0647
Cyanoalkylation of Imines Catalyzed by a Chiral Palladium Pincer Complex

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0648
Copper-Catalyzed Asymmetric Annulation

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Metal-Mediated Synthesis
z649
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0649
Direct Difluoroethylation of Hetero-aromatics, Michael Acceptors and Thiols FREE ACCESS

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0650
Photo- and Base-Promoted Direct C–H Arylation

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0651
Copper-Catalyzed Oxidative Cross-Coupling of Sulfoximines and Alkynes

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0652
Copper-Mediated Fluorination of Aryl Stannanes and Aryl Trifluoroborates

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0653
Iridium-Catalyzed C–H Borylation of Cyclopropanes

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0654
Palladium-Catalyzed Synthesis of N-Aryl Carbamates

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0655
Asymmetric Synthesis of α-Heterocyclic Tertiary Boronic Esters

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0656
Trifluoromethylation of Allylsilanes

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0657
Construction of all-cis-Octatetraenes

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0658
Iron-Catalyzed Alkene Hydroboration

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0659
Boron-Mediated Asymmetric Aldol Reaction

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0660
Copper-Catalyzed Hydrodefluorination of Fluoroarenes

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0661
Ag-Promoted, Pd-Catalyzed Intramolecular Direct Arylation of Cyclopropanes

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0662
Silver-Mediated Stereoselective Nitration of Mono- and Disubstituted Olefins

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0663
Titanocene-Catalyzed Dehydroxylative Cross-Coupling

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Organo- and Biocatalysis
z665
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0665
Biocatalytic Reductive Amination

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0666
Asymmetric Henry Reaction Catalyzed by Planar-Chiral Cyclophane Thiourea

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0667
Asymmetric Organocatalytic Thio-Diels−Alder Reactions

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0668
Catalytic Asymmetric Diaziridination

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0669
A Catalytic Asymmetric Acetalization

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0670
NHC-Catalyzed Diastereoselective Synthesis of Substituted Coumarins

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0671
Metal-Free Oxidative Coupling of Tertiary Amines to Ketones

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0672
Aminocatalytic Addition of Acetaldehyde to Activated Ketones

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Polymer-Supported Synthesis
z673
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0673
Benzylic Oxidation with Nano-MnO₂

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0674
Reduction of Nitrobenzenes and Nitroalkanes with NH₃·BH₃ using Au/TiO₂

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0675
Suzuki Coupling Using Co/C MNPs-Immobilized Dendritic Phosphine–Pd FREE ACCESS

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0676
Synthesis of Alkylboronates with Silica-SMAP/Ir Complex

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0677
Hydroamination of Alkynes by Au/TiO₂-N and Visible Light

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0678
N-Alkylation of Ammonia or Amines with Alcohols Using NiCuFeO_x

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0679
Intramolecular O-Arylation with a Polymeric Benzimidazolium Catalyst

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0680
Nano-Silica-Supported Palladium Nanoparticles for C–C Couplings

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0681
The Suzuki–Miyaura Coupling Catalyzed by SiO₂-Tripodal-DPPP-Pd

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0682
CuFe₂O₄-Catalyzed Etherification and Thioetherification of Aryl Halides

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0683
WO₃-Catalyzed Oxidation of Amines to Oximes using O₂

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0684
Nucleophilic Substitution Using Alkali Metal Salts Promoted by PSpentaEG

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0685
Synthesis of Pyrroles via Paar–Knorr Reaction Using TiO₂–SO₄^2–

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