Synfacts

Issue 12 · December 2013

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A145
SYNFORM ISSUE 2013/12
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Synthesis of Natural Products and Potential Drugs
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1255
Synthesis of Nafoxidine via Copper-Catalyzed Carboarylation
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1256
Synthesis of Maoecrystal V

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1257
Total Synthesis of (±)-Merochlorin A
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1258
Divergent Approach to Lycopodium Alkaloids

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1259
Synthesis of (–)-Minovincine

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1260
Total Synthesis of Ecteinascidin 743

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1261
Synthesis of the JAK2 Kinase Inhibitor AZD1480

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1262
Synthesis of an MDM2 Inhibitor

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1263
Total Synthesis of (+)-Neoxaline

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1264
Total Synthesis of (±)-Neofinaconitine

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1265
Formal Synthesis of Clopidogrel (Plavix^®)

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1266
Synthesis of All Four Reboxetine Stereoisomers

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Synthesis of Heterocycles
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1267
Diels–Alder Reaction–Fragmentation of Pyridinium Salts and Alkynes
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1268
Synthesis of 2-Fluoropyrroles from gem-Difluorocyclopropyl Ketones

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1269
Gold-Catalyzed Synthesis of Furan-3-ones via [2,3]-Sigmatropic Rearrangement

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1270
Synthesis of Imidazoquinolone Carbonitriles from Tetracyanoethylene

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1271
Rh(III)-Catalyzed Regioselective C–H Activation Route to Naphthyridinones

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1272
Metalation of 7-Azaindoles

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1273
Silver-Catalyzed Synthesis of Oxindoles

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1274
Radical Spirocyclization Route to Spirooxindoles

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1275
Pyrrolo[2,3-d]pyrimidines Through Activation of N-Benzyl Groups by Distal Amides

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1276
Pd-Catalyzed C–H Activation Route to Hydroxy Isoindolones

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1277
Synthesis of Pyrido[1,2-b]indazoles from the Reaction of 2-Arylpyridines with NaN₃

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1278
Ag-Catalyzed [5+2]-Cycloaddition Route to Dihydroazepines

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1279
Synthesis of Substituted Coumarins from Propargyl Vinyl Ethers

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1280
Rhodium-Catalyzed Synthesis of Benzazepinones

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1281
Efficient Heteroannulation Route to 2-Trifluoromethyl Quinolines

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Synthesis of Materials and Unnatural Products
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1283
A New Building Block for Low Band Gap Polymers

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1284
An Additional Path to [8]Circulenes

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1285
Diazo Compounds from Azides in Water

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1286
New Approach to the Synthesis of Thienoacenes

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1287
Template-Assisted Polymerization Leads to Polymers with Narrow Polydispersity

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1288
Dialumene-Benzene as a Synthon for Reactive Dialumenes

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1289
Rapid Access to BN-Containing Heptacene Isomers

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1290
Regioselective Direct Alkoxylation of Azobenzenes

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1291
Dibenzosilaborins: A New Class of Heterocycles

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1292
Expanding Cyclopropenes to Bifurans

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1293
Tandem Synthesis of Benzo[b]carbazoles

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1294
Efficient Synthesis of Dibenzohelicenes

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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1295
Diastereoselective Hydroxytrifluoro-methylation of Dienes Catalyzed by Copper

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1296
Binary Acid Catalysis for Asymmetric [4+2]-Cycloaddition Reactions

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1297
P-Chirogenic Organocatalysts in the Enantioselective Aza-MBH Reaction

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1298
Bifunctional Catalyst: Asymmetric Aldol Reaction Catalyzed by Amino Acid Salts

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1299
An S₂N₂ Ligand for Ru-Catalyzed Asymmetric Hydrogenation of Ketones

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1300
Enantioselective Dibromination of Allylic Alcohols by a Titanium Catalyst

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1301
Enantioselective Alkylation of Aldehydes with Zinc–2-Pyridylsulfinamides

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1302
Iridium-Catalyzed Asymmetric Direct Reductive Amination

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1303
Bis(oxazolidine)pyridine Ligands for Asymmetric [3+2] Cycloadditions

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1304
Enantioselective Palladium-Catalyzed α-Arylation of Amides

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1305
Cu-Catalyzed Enantioselective Alkynylation of Aldehydes

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1306
From Enals to Chiral γ‑Amino Alcohols via Asymmetric β-Borylation of Enimines

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1307
Spiroindolenines via a Ru-Catalyzed Intramolecular Allylic Dearomatization

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1308
Enantioselective Palladium-Catalyzed Allylic Dearomatization

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1309
Rh-Catalyzed Olefin Isomerization to Z-Configured α,β-Unsaturated Ketones

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1310
Silver-Catalyzed Conjugate Addition of Glycine Imino Esters

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1311
Rh-Catalyzed Asymmetric [2+2+2] Cycloadditions of Diynes with Isocyanates

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1312
Copper-Catalyzed Stereoselective Henry Reaction

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1313
Catalytic Enantioselective N-Sulfonyliminium Cyclization Cascade

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1314
Synthesis of Chiral 1,2-Diols via α-Hydroxyacetate Aldol Reaction

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1315
Diastereo- and Enantioselective Ni(II)-Catalyzed Alkylation Reactions

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1316
Cu(II)-Catalyzed Diastereo- and Enantioselective Synthesis of Pyrrolidines

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1317
Enantioselective Rhodium-Catalyzed Formal [4+3] Cycloaddition

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1318
DKR of Homoallylic Alcohols Using a Lipase and a Ruthenium Catalyst

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1319
Copper-Catalyzed Asymmetric Hydrogenation of Ketones

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1320
Haloamination of 3-Alkenyl-oxindoles and Chalcone Derivatives

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1321
Enantioselective Cobalt-Catalyzed Addition of Allenes to Silylacetylenes

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1322
TRIP-Catalyzed Asymmetric Allylation of Aldehydes

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1323
Copper-Catalyzed Enantioselective B–H Insertion Reactions

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Metal-Mediated Synthesis
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1325
Fluorination of Aryl Trifluoroborates
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1326
Novel Route to Arylsulfones Based on Diaryliodonium Salts

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1327
Pd-Catalyzed Alkynylation with Potassium Alkynyltrifluoroborates

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1328
Synthesis of γ-Substituted Butanolides from Cyclopropane Hemimalonates

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1329
Pd-Catalyzed Carbonylative Coupling of Aryl Halides and Potassium Malonates

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1330
Ni(II)-Catalyzed Arylmagnesiation of Alkynes

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1331
Arylation of Amino Acid Enolates

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1332
Cu-Catalyzed Intermolecular Regioselective Hydroamination of Styrenes

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1333
Conjugated Allyl Alcohols through One-Carbon Homologation of Aryl Epoxides

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1334
Amide Synthesis via MnO₂-Promoted C–H Activation of Methylarenes

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1335
Iron-Catalyzed Homocoupling Reaction of Aryllithium Reagents

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1336
Pd-Catalyzed β-Arylation of Silyl Ketene Acetals

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1337
Zinc-Mediated Synthesis of 1,5- and 1,4,5-Substituted 1,2,3-Triazoles

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1338
A General, Pd-Catalyzed Cyanation of (Hetero)Aryl Chlorides and Bromides

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1339
Synthesis of Benzothiophenes and Benzoselenophenes Mediated by Copper

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Organo- and Biocatalysis
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1341
Bis(amino)cyclopropenylidenes as Alternatives to NHCs in the Stetter Reaction

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1342
Bis(guanidino)iminophosphorane-Catalyzed Amination of Ketones

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1343
Organotextile Catalysis

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1344
Isothiourea-Catalyzed Pyridine Synthesis

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1345
Organocatalytic C–H Cross-Biaryl Coupling

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1346
Asymmetric Synthesis of Tertiary Thiols from 5H-Thiazol-4-ones and Nitroolefins

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1347
A Highly Enantioselective Route Towards α-Methylated Amines

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1348
Asymmetric Organocatalysis with Masked Acyl Cyanides

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1349
Disulfonimide-Catalyzed Asymmetric Synthesis of β³-Amino Esters

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1350
Organocatalytic Enantioselective Decarboxylative Aldol Reaction

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1351
Enantioselective Sulfonation of Enones by Cooperative Multicatalysis

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Polymer-Supported Synthesis
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1353
Flow Synthesis of Olanzapine

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1354
One-Pot Knoevenagel Condensation–Hydrogenation with a Nano-Pd Catalyst

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1355
Asymmetric Ring-Opening of meso-Epoxides with a Chiral Metal-Organic Framework
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1356
Cu-Catalyzed C–N Coupling in Water with a Polystyrene-Supported Ligand

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1357
Synthesis of Tetrasubstituted Pyrroles with H₂WO₄/SiO₂

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1358
Synthesis of Nitroalkenes with Polymer-Supported Triphenylphosphine

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1359
Cyclization–Cleavage Strategy for the SPS of Cyclic Peptides

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1360
Preparation of 2,2′-Biphenols via Suzuki–Miyaura Coupling with Pd/C

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1361
Selective Hydrogenation of Nitrobenzenes with Iridium Nanoparticles

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1362
Friedländer Quioline Synthesis Promoted by Chitosan-SO₃H

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1363
ortho-Benzoylation of Phenols Using Fe₃O₄ Nanoparticles

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1364
Oxidative Cross-Dehydrogenative Coupling with CuFe₂O₄ NPs

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