Synfacts

Ausgabe 02 · Februar 2014

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A17
Zanda, Matteo: SYNFORM ISSUE 2014/02 FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
z111
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0111
Synthesis of (S)-Sitagliptin FREIER ZUGRIFF

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0112
Total Synthesis of (+)-Methyl N-Decarbomethoxychanofruticosinate

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0113
Biogenetically Inspired Synthesis of Indole Alkaloids FREIER ZUGRIFF

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0114
Total Synthesis of Montanine-Type Alkaloids

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0115
Synthesis of a Glucokinase Activator

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0116
Total Synthesis of (±)-Gephyrotoxin

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0117
Synthesis of Diaryl Sulfones: GSK 742457

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0118
Synthesis of Thuggacin B

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0119
Synthesis of Voriconazole

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0120
Synthesis of GSK2263167

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0121
Synthesis of Renin Inhibitor DS-8108b

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0122
Synthesis of (±)-Sculponeatin N

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0123
Synthesis of Safingol

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0124
Synthesis of (+)-Bermudenynol

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Synthesis of Heterocycles
z125
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0125
Heteroannulation Route to Benzofurans

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0126
Three-Component Synthesis of Rhodanines on Nanoporous Silica

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0127
Synthesis of Benzofuranones from Alkynyl Aryl Ethers

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0128
Transformation of Sulfonylpyrroles into 6-Azaindoles

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0129
Iron(III) Chloride Catalyzed Synthesis of Spirocyclic Pyrimidinones

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0130
Ir(III)/Bi(OTf)₃-Catalyzed Prins Route to Pyran-Fused Indoles

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0131
Synthesis of Substituted Thiophenes from Polyhalogenated Nitrobutadienes

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0132
Palladium-Catalyzed Heteroannulation Route to 3-Trifluoromethylbenzofurans

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0133
Rhodium-Catalyzed Synthesis of Furo[2,3-b]pyran-6-ones

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0134
Synthesis of 2,5-Dihydrofurans via a Petasis Borono-Mannich Reaction

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0135
Rhodium-Catalyzed ortho-C–H Acylation Route to 3-Alkylidenephthalides

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0136
Synthesis of 1,3-Thiazin-2-ones via an Asymmetric Hetero-Diels–Alder Reaction

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0137
Asymmetric Organocatalytic Synthesis of 2,6-Diazabicyclo[2.2.2]octanones

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0138
C4-Alkenylation of 3-Formyl Indoles via Ruthenium(II)-Catalyzed C–H Activation

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0139
Synthesis of Piperazines via Gold-Catalyzed Cyclization of Propynyl Diamines

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Synthesis of Materials and Unnatural Products
z141
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0141
Having a Hydrocarbon Ball

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0142
Aminyl Tetraradicals Persist at Room Temperature

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0143
Four-in-One: Pentafulvalenes via Quadruple Carbopalladation

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0144
Gold-Catalyzed Diastereoselective Synthesis of Naphtha[b]cyclobutenes

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0145
Zipping Up Thienylbenzenes to Thia[7]helicenes

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0146
Two Stable Extended Zethrenes

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0147
A Stable, Intra-Sheet π-Conjugated Covalent Organic Framework

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0148
A New Record for Proton Sponges

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0149
A π-Extended Indenofluorene with Substantial Singlet Biradical Character

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0150
Tetracenes in a Bowl-Shaped Arrangement

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0151
Programmed Synthesis of Arylthiazoles

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0152
High Yielding Synthesis of meso-Substituted Macrocycles

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0153
A Simple Reagent for the Difluoroethenylation of Arenes

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z155
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0155
Asymmetric Allylic Alkylation of Acyclic β‑Keto Esters Catalyzed by Iridium FREIER ZUGRIFF

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0156
Asymmetric Addition of Phosphines Catalyzed by P-Chiral Pd Complexes

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0157
Enantioselective [3+2] Annulation via C–H Activation Catalyzed by Iridium FREIER ZUGRIFF

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0158
Enantioselective Hydrogenation of Nitroolefins by Rhodium Catalysis

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0159
[3+3] Cycloaddition of Azomethine Ylides with Azomethine Imines FREIER ZUGRIFF

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0160
Synthesis of Axially Chiral Biaryls by a Palladium Catalyst

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0161
Asymmetric Ring Opening of Oxabenzonorbornadiene with Amines

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0162
Asymmetric Synthesis of QUINAP via Atropselective C–P Coupling

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0163
Iron–Schiff Base Catalyzed Asymmetric Hydrophosphonylation

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0164
Asymmetric [3+2] Cycloaddition of Disubstituted Nitroalkenes

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0165
Kinetic Resolution of Racemic Propargyl Acetates by Palladium Catalysis

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0166
Yttrium-Catalyzed Asymmetric Aldol Cyclization of α-Keto Esters

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0167
Asymmetric Synthesis of 1,2,4-Triazinane Frameworks by Copper Catalysis

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0168
Enantioselective Copper-Catalyzed Oxytrifluoromethylation of Alkenes

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0169
Enantioselective Synthesis of γ-Methyl-Substituted Carbonyl Compounds

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0170
Asymmetric Sulfoxidation Catalyzed by Mn/Porphyrin

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0171
Asymmetric Synthesis of Axially Chiral Biaryls via [2+2+2] Cycloaddition

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0172
Co(II)-Based Metalloradical Catalysis for Asymmetric Cyclopropanation

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0173
Asymmetric Reduction of 2,2-Dimethyl-4-dioxinones Catalyzed by Ruthenium

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0174
Copper-Catalyzed Enantioselective Intramolecular Cannizzaro Reaction

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0175
Subsequent Reduction and Jocic-Type Reaction of Trichloromethyl Ketones

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0176
Ir-Catalyzed Asymmetric Hydrogenation and Transfer Hydrogenation of Ketones

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0177
Rhodium-Catalyzed Enantioselective Hydrogenation of 1-Alkylvinyl Benzoates

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0178
Deoxycholic Acid Derived Biaryl Phosphites in Conjugate Addition

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0179
[3+3] Cycloaddition of Enol Diazoacetates with N-Acyliminopyridinium Ylides

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0180
Asymmetric Conjugate Addition of Arylboronic Acids to Nitroolefins

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0181
Dehydrogenative Cross-Coupling of Simple Alkenes and Acrylates

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0182
Bisheterocyclizations of Alkynes Catalyzed by Platinum

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0183
Iron-Catalyzed Asymmetric Ring Opening of meso-Epoxides

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Metal-Mediated Synthesis
z185
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0185
N–Bpin-Directed Borylation of (Hetero)Aryls FREIER ZUGRIFF

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0186
Fluorination of Aryl Trifluoroboronates with Potassium Fluoride Mediated by Copper

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0187
Enantiospecific Transition-Metal-Catalyzed Allylic Alkylation

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0188
1,4-Reductive Aldol Reactions of Substituted α,β-Unsaturated Amides

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0189
Reductive Coupling and Reduction of Barbituric Acids Using SmI₂

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0190
Allylation of N-(Quinolin-8-yl)benzamides with Allyl Ethers Catalyzed by Iron

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0191
Cyanotrifluoromethylation of Styrenes Using the Togni Reagent and Copper Cyanide

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0192
Electrophilic Difluoro(phenylthio)methylation of Allyltrimethylsilanes

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0193
gem-Difluoroolefination of Diazo Compounds with TMSCF₃ Catayzed by Copper

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0194
Cross-Coupling of Silanes with Organic Halides Catalyzed by Copper

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0195
Reactions of 2-Pyrone Derivatives with MeMgBr Catalyzed by Iron

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0196
Synthesis of 2-Boryl 1,3-Butadienes from α-Alkoxy Allenes Catalyzed by Copper

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0197
Substitution of Unactivated Alkyl Fluorides Using YbI₃

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0198
Base-Dependent Enantiodivergent De-protonation/Acylation of α-Amino Nitriles

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0199
One-Pot Synthesis of Polysubstituted Isochromanes

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Organo- and Biocatalysis
z201
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0201
β-Substituted α-Hydroxy Esters via Dynamic Kinetic Resolution

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0202
Boronate Ester Assisted Chiral Carboxylic Acid Catalyzed Aziridination

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0203
Direct β-Functionalization of Ketones by Photoredox-Coupled Organocatalysis

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0204
A Chiral Tertiary Amine Catalyzed Intermolecular [3+2] Annulation

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0205
Conjugate-Base-Stabilized Brønsted Acids in Asymmetric Catalysis

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0206
An Organocatalytic Route towards Annulated Indoles

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0207
Axially Chiral Amine Catalyzed Asymmetric Hydroxyamination of Aldehydes

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0208
Organocatalytic Remote Activation in an Aza-Diels–Alder Reaction

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0209
Asymmetric Counteranion-Directed Photoredox Catalysis

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0210
Two Fluorinated Compounds from One Organocatalytic Kinetic Resolution

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0211
Asymmetric Catalytic α-Benzylation of Aldehydes

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0212
Asymmetric Synthesis of Pyrroloindolones by N-Heterocyclic Carbenes

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Polymer-Supported Synthesis
z213
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0213
Click Reaction with Copper(I)–NHC Supported on Fe₃O₄/Si

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0214
Asymmetric Hydrogenation of Ketones with a PMO-Supported Rhodium Complex

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0215
PS-PAr₃ Hybrid: Metal Complexation and Catalytic Applications FREIER ZUGRIFF

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0216
Direct Amidation from Alcohols and Amines with Polymeric Au or Au/Co

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0217
Photocatalyzed Deoxygenation of Styrene Oxides Using TiO₂

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0218
Strecker and Kabachnik–Fields Reactions with DHAA/Fe₃O₄

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0219
Asymmetric Aldol Reaction Using a Polymeric Hydantoin Auxiliary

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0220
Flow Oppenauer Oxidation of Alcohols with Zirconia Oxide

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0221
Glassy Carbon-Supported Rhodium(I) Catalysts for Intramolecular Hydroamination

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0222
Enantioselective Aldol Reaction in Water with a Supported Prolinamide

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0223
Synthesis of Benzoyl Fumarates with Supported Nicotinic Acid Thioester

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0224
Aerobic Oxidation with Branched Polystyrene-Supported Gold NPs

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