Synfacts

Issue 05 · May 2014

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Synform
A59
Zanda, Matteo: SYNFORM ISSUE 2014/05 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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0447
Total Syntheses of Ampelopsin D, Pallidol, and Quadrangularin A FREE ACCESS

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0448
Total Synthesis of Caraphenol A

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0449
Synthesis of SMO Inhibitor PF-04449913 FREE ACCESS

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0450
Total Synthesis of (±)-Mersicarpine

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0451
Total Synthesis of Guttiferone A

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0452
Synthesis of an Estrogen-Related Receptor 1 Inhibitor

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0453
Synthesis of a TRPV1 Antagonist

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0454
Synthesis of Dantrolene

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0455
Total Synthesis of (+)-Tubingensin A

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0456
Synthesis of (±)-Sorbiterrin A

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0457
Synthesis of Podophyllotoxin

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Synthesis of Heterocycles
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0459
[3+2] Cycloaddition Route to Spirooxindoles

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0460
Synthesis of 1,2-Benzisoxazoles by Palladium-Catalyzed [4+1] Annulation

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0461
Synthesis of Trisubstituted Oxazoles via a Three-Component, One-Pot Reaction

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0462
Efficient C–C Aryl–Heteroaryl Bond Formation by Photoredox Direct Arylation

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0463
Pyrroles via Copper-Promoted Oxidative Coupling of Enamides with Alkynes

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0464
Construction of Fused Pyrroles from 1,3-Diones and N-Alkynylhydroxyamines

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0465
Rhodium-Catalyzed Synthesis of Polysubstituted Indoles from Styryl Azides

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0466
Synthesis of Functionalized Pyrroles by a Multi-Component Reaction

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0467
One-Pot Asymmetric Synthesis of 2,3-Dihydropyrroles

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0468
Ruthenium-Catalyzed Synthesis of Lactams from Cyclic Amines and Water

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0469
Rhodium-Catalyzed Synthesis of β-Naphthols and Indenes

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0470
Synthesis of Spiromorpholinotetra-hydropyrans Through a Prins Bicyclization

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0471
Oxa- versus Thia-Selectivity in the Prins Cyclization

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0472
Transition-Metal-Free Synthesis of 1,4-Benzodiazepinones

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Synthesis of Materials and Unnatural Products
z473
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0473
Extending Arenes via C–H Activation with Rhodium FREE ACCESS

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0474
It Takes 2+2+2 to Tango

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0475
Chalcogen α and ω End Groups on P3HT

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0476
[5]Cycloparaphenylene: The Smallest Nanohoop

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0477
Flying π: ‘Flapping’ Aceneimides with Cyclooctatetraene Cores

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0478
Easy as 1, 2, 3: Cyclization to Afford N²-Substituted Benzotriazoles

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0479
Fun with [5]Cumulenes and Tetracyanoethylene

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0480
Münching up Fullerenes Asymmetrically

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0481
Cyclizations with Transient Sulfenic Acids

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0482
Alkynes Made-to-Order with Light, in Air and Water

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0483
Selective C–H Arylation of Fluorinated Heterocycles

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z485
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0485
Copper-Catalyzed Diastereoselective Synthesis of Amino Azides

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0486
Asymmetric Construction of Alkenyl-Substituted Quaternary Carbons

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0487
Asymmetric Friedel–Crafts Reaction Using a Chiral-at-Metal Iridium Catalyst FREE ACCESS

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0488
Stereodivergent Synthesis of Labile Aldehydes via a Dual Catalysis Approach

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0489
Asymmetric Iridium-Catalyzed Allyl–Alkene Coupling en route to Chiral 1,5-Dienes FREE ACCESS

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0490
Ruthenium–BINAP Catalytic Hydrogenation on Multikilogram Scale

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0491
Chiral Sulfoxide-P Ligands for Palladium-Catalyzed Asymmetric Allylic Alkylation

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0492
Asymmetric Zinc-Catalyzed Aldol Reaction of Glycinate Schiff Bases and Aldehydes

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0493
Iridium-Catalyzed Intramolecular Asymmetric C–H Functionalization of α-Keto Amides

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0494
Diastereoselective Synthesis of N-Sulfonyl α,β-Diamino Acid Derivatives

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0495
Rhodium-Catalyzed Addition of Arylboronic Acids to Alkenylazaarenes

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0496
Asymmetric Imino Diels–Alder Reaction with an Inverse Electron Demand

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0497
Copper-Catalyzed Asymmetric Friedel–Crafts Alkylation of Indoles

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0498
Synthesis of β^2,2-Amino Acids via Asymmetric Friedel–Crafts Alkylation

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0499
Copper-Catalyzed Enantioselective Synthesis of β-Hydroxy-α-amino Acids

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0500
Rhodium–Diene Complex Catalyzed Asymmetric Alkenylation

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0501
Synthesis of (–)-Aurantioclavine via Intramolecular Allylic Amination

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0502
Chiral MOF Catalyst for Asymmetric Cyanation of Aldehydes

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0503
Diastereoselective Sequential Aldol Reaction of Disilyl Enolether

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0504
Copper-Catalyzed Enantioselective Addition of Nitromethane to 2-Acylpyridine N-Oxides

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0505
Copper-Catalyzed Stereoselective Synthesis of (Borylmethyl)cyclopropanes

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0506
Asymmetric Hydrogenation of Ketones by Ruthenium Catalysis

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0507
Asymmetric Synthesis of 1,3-Dioxolanes via [3+2] Cycloaddition

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0508
Rhodium-Catalyzed Insertion of Carbenes into Benzocyclobutenols

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0509
Ruthenium-Catalyzed Asymmetric Allylic Amination

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0510
Asymmetric Hydrocyanation Using Ru(phgly)₂(binap)–MeOLi System

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0511
Rhodium Furanoside Monophosphite Catalyzed Asymmetric Hydrogenation

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0512
Enantioselective Four-Component Cascade Reaction of Aryldiazoesters

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0513
Hydrosilylation of Ketones Catalyzed by Zn–TPS-he-pybox

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Metal-Mediated Synthesis
z515
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0515
Stereospecific Kumada Cross-Coupling of Alkyl and Aryl Grignards FREE ACCESS

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0516
Zinc-Catalyzed Borylation of Alkyl Halides

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0517
O-Arylation of Functionalized Phenols Using Substituted Arylbismuth Reagents

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0518
α-Siladifluoromethylation of Lithium Enolates Using TMSCF₃

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0519
Synthesis of Enantiomerically Enriched Cyclohexanones

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0520
ortho-Alkylation and Arylation of Fluoroaryl Imines

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0521
C–H Activation of Heterocycles Using an Imine Directing Group

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0522
Generation of 3,3-Bis(silyl) Allyloxy Lithium for syn-Addition to Aldehydes and Ketones

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0523
Synthesis of Unsymmetric Aryl Aryl Ketones Using Acylindium Reagents

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0524
Controlled α- and β-Arylation of Boc-Protected Amines

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0525
Copper-Catalyzed α-Amination of Phosphonates and Phosphine Oxides

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0526
Synthesis of 2-Substituted 2-Azetines by Lithiation of N-Boc-2-azetines

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0527
Reduction of Amides to Alcohols Using SmI₂

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0528
Direct Trifluoromethylation of Coumarins Mediated by Manganese(III)

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Organo- and Biocatalysis
z529
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0529
Organocatalytic Asymmetric Formation of Steroids

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0530
Kinetic Resolution of BINAM Derivatives Catalyzed by a Brønsted Acid

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0531
Proline-Catalyzed Asymmetric N-Nitroso Aldol Reactions

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0532
Phase-Transfer-Catalyzed Asymmetric α-Arylation of α-Amino Acid Derivatives

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0533
Diels–Alder/Lactonization Cascade Reactions

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0534
Asymmetric Cooperative Catalysis in N–H Insertion Reactions

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0535
Aminocatalytic Asymmetric Alkylation of Ketones

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0536
Isothiourea-Catalyzed Asymmetric [2,3]-Rearrangement of Ylides

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0537
Intramolecular Organocatalytic Oxidative Cyclization

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Polymer-Supported Synthesis
z539
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0539
Hydroboration of Alkynes with Copper Powder

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0540
Transamidation of Amides Catalyzed by Fe-Mont

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0541
Formylation of Aryl Iodides with CO₂ Using Palladium on Carbon FREE ACCESS

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0542
Carbonylative Suzuki–Miyaura Coupling with in situ Generated Pd Nanoparticles

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0543
Click Reaction with Cu(II)-Triazine Dendrimer Immobilized on Nanosilica

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0544
Asymmetric Hydrogenation of Ketones Using a Fe₃O₄-Supported Rhodium Complex

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0545
Flow Hydration of Nitriles with Manganese Dioxide

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0546
A Resin-Bound Phosphoric Acid Catalyst: Asymmetric Flow Reactions

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0547
Hydrogenation of Aldehydes Using Phosphine Oxide Stabilized Gold Nanoparticles

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0548
Mesoporous Niobium Oxide Sphere Catalyzed Transamidation Reaction

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0549
Resin-Bound Triazenes for the Synthesis of Hydrazone Derivatives

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0550
Formylation of Amines with DMF Using CeO₂

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Erratum
0551
Singer, R. A.: Synthesis of Axitinib

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0551
Yang, W.; Sun, J.; Xu, X.; Zhang, Q.; Liu, Q.: Synthesis of Benzisoxazolones by Ruthenium and Copper Catalysis

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0552
Pace, V.; Rae, J. P.; Procter, D. J.: Copper-Catalyzed Enantioselective 1,4-Conjugate Silyl Additions

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