Synfacts

Issue 04 · April 2015

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SYNFORM ISSUE 2015/04 FREE ACCESS

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Synthesis of (±)-Aureol

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Synthesis of PLK4 Inhibitor CFI-400945 FREE ACCESS

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Synthessis of Tipifarnib

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Synthesis of Pseudopterosin (–)-G-J Aglycone

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0348
A Claisen Approach to 4′-Ed4T

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Synthesis of Trioxacarcin DC-45-A2

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0350
Synthesis of an HCV Protease Inhibitor

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0351
Synthesis of (−)-Nardoaristolone B

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0352
Assembly-Line Synthesis of (+)-Kalkitoxin and (+)-Hydroxyphthioceranic Acid

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0353
Divergent Synthesis of Monoterpene Indole Alkaloids

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0354
Synthesis of the Hydroxyquinolinone Core of β2-Receptor Agonists

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0355
Synthesis of Taxadienone

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Synthesis of Heterocycles
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0357
Atom-Efficient Organolanthanide 1,2-Dearomatization of Pyridines

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0358
Arene–Ynamide Cyclization Approach to Pyrroloquinolines

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0359
Imidazoles and Imidazoliums from Propargylamines and Isonitriles

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0360
Diastereoselective Synthesis of Fluorinated Amino-Sugars

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0361
Synthesis of Fused Indoles and Pyridin-2-ones by Radical Cyclization Cascades

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0362
Synthesis of Polyfluoro-1,3-thiazine Derivatives

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0363
Preparation of Pyrido[3,4-d]azepines by Pyridine Ring Heteroannulation

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0364
Synthesis of Dihydropyrazines from N-Sulfonyl-1,2,3-triazoles and Aziridines

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0365
Palladium-Catalyzed Heteroannulation Route to Azaindoles

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0366
Rhodium-Catalyzed Directed Halogenation of π-Excessive Heterocycles FREE ACCESS

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0367
Sultams by Arylation of Cyclic N-Sulfonyl Aryl Alkyl Ketimines

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0368
Ruthenium-Catalyzed Synthesis of 1,4-Benzodiazepines

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0369
Seven-Membered Heterocycles by Chlorosilane-Catalyzed Heteroannulation

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0370
Synthesis of Enantioriched δ-Lactones from β-Halo-α-keto Esters

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0371
Rhodium-Catalyzed Oxidative Annulation Route to 1-Aminoindolenines

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Synthesis of Materials and Unnatural Products
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0373
Carbo-Quinoid Carbo-Benzene Switch

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0374
Convenience is King: One-Pot Derivatization of Azulenes

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0375
Hexaarylbenzenes with Five or Six Distinct Substituents

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0376
No Metal, No Problem: Transition Metal Free ROMP

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0377
Silylation of Aromatic Heterocycles with Potassium tert-Butoxide Catalyst

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0378
Decorate it with Sulfur

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0379
Climbing the Ladder

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0380
Modular Synthesis of [6]Polynorbornane-Based Ligands

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0381
SET Yourself Up for Some Fast, Cheap, and Easy Phenanthrenes

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0382
One-Pot Reactions to Make Indolos? YOLO

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0383
Dialkylzinc-Mediated Perfluoroalkylation

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0384
Finding Propellers Among the Cascades

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z385
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0385
Enantioselective and Stereodivergent Synthesis of β,β-Diaryl-α-Amino Acids FREE ACCESS

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0386
Enantioselective Gold-Catalyzed Cyclopropanation

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0387
Ruthenium-Catalyzed Z-Selective Cross-Metathesis of Allylic Alcohols FREE ACCESS

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0388
Copper-Catalyzed Asymmetric β-Boration of α,β-Unsaturated Esters

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0389
Aryl Esters as Electrophiles in Nickel-Catalyzed Asymmetric α-Arylation

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0390
Copper-Catalyzed Enantioselective Hydroboration of Strained Alkenes

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0391
Isomerization of Terminal Alkenes to (Z)-2-Alkenes via Cobalt Catalysis

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0392
Nickel-Catalyzed Enantioselective Reductive Cyclizations of Alkynones

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0393
Palladium-Catalyzed Enantioselective Dearomative Cyclization of Phenols

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0394
Palladium-Catalyzed Enantioselective Hydrogenolysis of N-Sulfonyloxaziridines

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0395
Diastereoselective Synthesis of Highly Substituted Indolines via Palladium Catalysis

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0396
Palladium-Catalyzed Desymmetrization of meso-Diols

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0397
Magnesium-Catalyzed Stereoselective Dearomatization of β-Naphthols with Aziridines

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0398
Asymmetric Hydrogenation Catalyzed by Chiral Alkenylboranes

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0399
Rhodium-Catalyzed Asymmetric Isomerization of 4-Iminocrotonates

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0400
Direct Asymmetric Vinylogous Michael Addition Catalyzed by Ytterbium(III)

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0401
Asymmetric Hydroformylation of Vinylarenes via Rhodium Catalysis

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0402
Rhodium-Catalyzed Enantioselective Addition of Thiols to Allenes

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0403
Asymmetric Hydrogenation of Conjugated Enamides by Rhodium Catalysis

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0404
Asymmetric Synthesis of P-Stereogenic Phosphinamides via Pd(II) Catalysis

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0405
Palladium-Catalyzed Asymmetric Synthesis of α-Quaternary Mannich Products

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0406
Copper-Catalyzed syn-Selective Alkylboration of Alkynes

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0407
Asymmetric Synthesis of 5,6-Dihydrophenanthridines

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0408
Catalytic Asymmetric Pauson–Khand Reaction Using Cobalt

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0409
Enantioselective [3+2] Cycloaddition Catalyzed by Magnesium

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0410
Desymmetrization of Maleimide-Based Bis(alkynes) via Cu-Catalyzed Click Reaction

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0411
Zinc(II) Chloride Promoted Asymmetric Hydrogenation

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0412
Enantioselective Oxidative Coupling of 2-Naphthols and Aryl Methyl Ketones

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0413
Iron-Catalyzed Asymmetric Epoxidation of Electron-Poor Olefins

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Metal-Mediated Synthesis
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0415
Addition of Carboxylic Acids Using Chiral Lithium Amides as Auxiliaries FREE ACCESS

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0416
Stereoselective Alkylation of Malonate-Imidazolidinones

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0417
Stereoconvergent [1,2]- and [1,4]-Wittig Rearrangements

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0418
Iron-Catalyzed Boration of Alkynes

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0419
Tandem Arylation–Protodecarboxylation

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0420
trans-2,6-Disubstituted 5-Methyl-3,6-dihydropyrans by Zinc Catalysis

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0421
Phosphorylation of (Benzo)thiazoles Mediated by Silver Nitrate

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0422
Regioselective Derivatizations of a Benzamide Scaffold

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0423
Nickel-Catalyzed Alkynylation of Anisoles

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0424
Zirconium-Mediated Multicomponent Reactions of 1,3-Butadiynes

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0425
Palladium-Catalyzed α-Arylation of Aryl Acetic Acid Derivatives

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0426
Decomposition of Difluorocarbene for Trifluoromethylation

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0427
Trifluoromethylthiolation of Alcohols Using Silver(I) Trifluoromethanethiolate

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0428
Copper-Catalyzed Asymmetric Allylic Alkylation

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0429
Copper-Catalyzed Cross-Coupling of Epoxides with Arylboronates

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Organo- and Biocatalysis
z431
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0431
Hydroxylation of Aliphatic C–H Bonds with a Ketone-Derived Organocatalyst

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0432
NHC-Catalyzed Radical β-Hydroxylation of Enals

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0433
Enantioselective [5+2] Cycloaddition of Oxidopyrylium Ylides and Enals

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0434
Kinetic Resolution of 1,2-Amino Alcohols by Intermolecular Acetalization

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0435
Asymmtric Synthesis of Indanes by 5-endo-trig Cyclization

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0436
Reduction of Aryl Halides by Consecutive Two-Photon Excitation

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0437
Resolution of Racemic Diols by Asymmetric Acetalization

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0438
Organocatalytic Addition of Aldehydes to 4-Vinylpyridines and Vinylarenes

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Polymer-Supported Synthesis
z439
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0439
Hydration of Alkynes with Au/TiO₂ in the Presence of Morpholine

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0440
Amination of Aryl Halides Using CuSO₄@Chitosan

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0441
Flow-Generated Diazo Compounds and Their Use in Cross-Coupling FREE ACCESS

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0442
Hydrogenation of Nitroarenes Using a Carbon Nanotube–Ruthenium Nanohybrid

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0443
Carbene Transfer Reaction Using a PS-Supported Copper Catalyst

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0444
Selective Transfer Semihydrogenation of Alkynes Using AuNPore

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0445
Graphitic Carbon Nitride Promoted Photoredox Fluoroalkylation of Arenes

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0446
Synthesis of Pyrroles Using Supported p-Toluenesulfonic Acid

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0447
Dendritic-PEGylated γ-Fe₂O₃–PdNPs as Catalysts for C–C Bond Formations

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0448
Copper-MOF-Catalyzed Aerobic Oxidation of Olefins and Alcohols

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0449
A Ruthenium Catalyst for Coupling of Benzoic Acids with Internal Alkynes

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0450
C–H Arylation of Heteroarenes Using Fe₃O₄–CeO₂ Magnetite Nanoparticles

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0451
Carboxylation of Terminal Alkynes with Carbon Dioxide Using Ag@MIL-101

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0452
Ring-Closing Metathesis with an Ionic MNP-Supported Ru–Carbene Complex

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