Synfacts

Issue 07 · July 2015

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A90
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Total Synthesis of Paspaline

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Synthesis of Diterpenoid Steenkrotin A FREE ACCESS

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Synthesis of Aliskiren

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Synthesis of DZ-2384 FREE ACCESS

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Total Synthesis of Santalin Y

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Synthesis of rac-Efavirenz

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Formal Synthesis of Telaprevir

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Synthesis of 5,6-Dihydrocineromycin B

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0686
Synthesis of Mycoleptodiscin A

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0687
Synthesis of (+)-Muironolide A

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0688
Total Synthesis of (–)-Galanthamine and (–)-Lycoramine

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0689
Synthesis of a BACE1 Inhibitor

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Synthesis of Heterocycles
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0691
Rhodium(III)-Catalyzed Synthesis of 1,2-Benzothiazines

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Enantioselective Copper(I)-Catalyzed Construction of Spiroketals

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0693
6-endo-dig versus 5-exo-dig. The Profound Effects of Acetonitrile

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0694
Synthesis of Dihydropyridin-2-ones via an Ugi–Aldol Reaction

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0695
Minisci-Type Synthesis of Tetrahydropyridopyridazines

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0696
Single-Step Synthesis of Isoindolinones

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0697
Synthesis of Fluorinated Diphenylpyrazole

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0698
Four New Bonds in One Pot: Isoxazolines from Olefins and 2-Ethylquinolines

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0699
Pyrido[2,3-c]coumarins via an Intramolecular Povarov Reaction

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0700
Synthesis of 1,2-Borazaronaphthalenes

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0701
Benzyne Route to Benzothiazoles

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0702
Copper-Catalyzed Oxidative Annulation Approach to Oxadiazoles

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0703
Enamide Umpolung for the Synthesis of Heterocycles

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0704
Oxabicycles via Sequential Prins–Wagner–Ritter Processes

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0705
Synthesis of Hexahydropyrano[3,4-c]chromenes via Prins Bicyclization

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Synthesis of Materials and Unnatural Products
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0707
Hexaaza Macrocycles Revisited

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0708
Nestable Tetrakis(spiroborate) Nanocycles

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0709
Circulene Flow

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0710
A Mild Route to Quinoxalines Featuring Iodine

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0711
Tiny Molecule, Big Fluorescence

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0712
Synthesis of 2,5-Disubstituted Thiazoles

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0713
Phospholify and Diversify

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0714
Pitched Propeller PAHs

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0715
Bowled Over! Nitrogen Takes Center Stage from Carbon in Azacorannulenes

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0716
A Polymerization Displaying Great Tact

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0717
Incorporating More Nitrogen Atoms in Hexacenes

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0718
A Molecular Spring

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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0719
Copper Hydride Catalyzed Synthesis of 2,3-Disubstituted Indolines FREE ACCESS

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0720
Asymmetric Haloaminocyclization for the Synthesis of Cyclic Sulfamates

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0721
Rhodium-Catalyzed Asymmetric Dearomatization of Naphthols with Alkynes FREE ACCESS

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0722
Synthesis of Indanes and Indanones through Tandem Catalysis

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0723
Iridium-Catalyzed Branched-Selective Hydroarylation of Vinyl Ethers

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0724
Iridium-Catalyzed Asymmetric Hydrogenation of Ketones in Ethanol

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0725
Gold-Catalyzed [2+2+2] of Allenamides, Alkenes and Aldehydes

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0726
Catalytic Stereoselective Reaction of β-Lactams with Aldehydes

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0727
Palladium-Catalyzed Enantioselective Reductive Heck Reactions

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0728
Palladium- and Chiral Phosphoric Amide/Acid-Catalyzed C–H Arylation

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0729
Enantioselective Allylic Alkylation of Ortho-Substituted Cinnamyl Bromides

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0730
Enantioselective Synthesis of α-Trifluoromethylamines

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0731
Iron-Catalyzed Z-Selective Olefin Synthesis

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0732
Asymmetric Transfer Hydrogenation of Ketones by Macrocyclic Iron Complexes

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0733
Addition of Allenes to Fluorinated Alcohols Catalyzed by Ruthenium

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0734
Iridium-Catalyzed Intramolecular Asymmetric C–H Alkylations

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0735
Zirconium-Catalyzed Asymmetric Hydroamination of Primary Aminoalkenes

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0736
Enantioselective Scandium-Catalyzed 1,6-Addition of Oxindoles

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0737
Synthesis of 3-Tetrasubstituted Oxindoles by Using a Chiral Calcium Catalyst

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0738
Enantioselective Copper-Catalyzed Synthesis of Dispiropyrrolidines

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0739
Copper-Catalyzed Synthesis of CF₃-Substituted Oxazolines

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0740
Asymmetric Mannich-Type Reaction of Ketimines and Aminoacetonitriles

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0741
Formylation of Allylic Carbonates with Formaldehyde N,N-Dialkylhydrazones

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0742
Asymmetric Transfer Hydrogenation by Means of Nickel Catalysis

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0743
Diastereoselective Synthesis of cis-β-Fluorocyclopropane Carboxylates

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0744
Catalytic Synthesis of Vinylcyclopropanes by Intramolecular Cyclopropanation

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0745
Ring Enlargement of Alkynyl Donor–Acceptor Cyclopropanes

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0746
Palladium-Catalyzed Dynamic Kinetic Asymmetric Spiroannulation

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Metal-Mediated Synthesis
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0747
Rhodium-Catalyzed Asymmetric Cyclopropylation

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0748
Gallium-Promoted Halocyclization

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0749
Cobalt-Catalyzed Hydroboration of Alkynes FREE ACCESS

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0750
Synthesis of Fluoren-9-ones via Carbonylative C–C Bond Formation

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0751
Asymmetric Addition of Arylboronic Acids to Nitrostyrenes

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0752
1,4-Hydroboration of Pyridines

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0753
Synthesis of Vinyl Boronates

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0754
Iron(II)-Mediated C–N Bond Formation Towards 2-Aminothiazoles

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0755
Asymetric Nickel-Catalyzed Synthesis of Azetidines and Aziridines

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0756
Carbolithiation of Heterosubstituted Alkynes

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0757
Copper-Mediated Radical Trifluoromethylation

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0758
Trifluoromethylation of Substituted Arenes and Heteroarenes

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0759
Copper-Mediated Cyclization Approach to 3H- and 1H-Indoles

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0760
Desymmetrization of 1,1-Diborylalkanes via Suzuki–Miyaura Cross-Coupling

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0761
Grignard Addition to Aldimino Esters

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Organo- and Biocatalysis
z763
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0763
Enantioselective Intramolecular Aza-Diels–Alder Reactions

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0764
A Mild Neutral Silicon Lewis Acid for Hydro- and Cyanosilylations

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0765
Radical Alkylation of Aldehydes via Asymmetric Photo-Organocatalysis

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0766
Organocatalytic CO₂ Trapping Using Alkynyl Indoles

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0767
NHC-Catalyzed Benzannulation via 1,6-Addition to Conjugated Dienals

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0768
Quaternary Stereocenters via NHC-Catalyzed Sulfa-Michael Addition

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0769
Desymmetrizing Michael Reactions via Enol Catalysis

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0770
Facile Net Cycloaddition Approach to Optically Active 1,5-Benzothiazepines

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Polymer-Supported Synthesis
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0771
Silica-Supported Iridium Complex Catalyst for Asymmetric Allylic Amination

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0772
C–P Bond Formation Catalyzed by a Magnetic Nanoparticle-Supported Palladium Catalyst

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0773
A Cellulose-Supported DNA-Based Ligand for Asymmetric Catalysis FREE ACCESS

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0774
Cross-Coupling of Iodides with Nucleophiles by Using Copper Clusters

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0775
Aerial Oxidation of Alcohols on a Silica–γ-Iron(III) Oxide Supported Palladium Complex

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0776
Dendrimer-Encapsulated Palladium Nanoparticles for Flow Cross-Couplings

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0777
Aerobic Oxidation of Alcohols with Gold–Platinum/Polystyrene Nanoparticles

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0778
Deoxygenation of Carbonyls by Poly(methylhydrosiloxane) on Palladium/Carbon

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0779
Gold Nanoparticle Promoted Cycloisomerization of Alkynoic Acids

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0780
Huisgen Cycloaddition on a Polymer-Supported Copper Catalyst

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0781
Well-Defined Adenosine Diphosphate Ribose Oligomers

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0782
Double Carbonylation of Aryl Iodides with Amines on Palladium Nanoparticles

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0783
Dehydrogenation of Alcohols to Carboxylic Acids on Palladium/Carbon

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0784
Ruthenium-Catalyzed Oxidative Decarboxylation of Amino Acids

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0785
C–O and C–X Bond-Forming Reactions with Pd(II)/MWCNT

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