Synfacts

Issue 06 · June 2019

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A78
Zanda, Matteo: SYNFORM ISSUE 2019/06 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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0581
Enantioselective Total Synthesis of (–)-Ambiguine FREE ACCESS

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0582
Total Synthesis of (–)-Alstofolinine A

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0583
Formal Synthesis of Entecavir

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0584
Synthesis of (–)-Oxycodone

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0585
Syntheses of (+)-Akuammiline and (–)-Echitamine

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0586
Syntheses of (–)-Indoxamycins A and B

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0587
Synthesis of (±)-Chalcitrin

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0588
Synthesis of Cembrane Diterpenoids

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0589
Total Synthesis of Endiandric Acids FREE ACCESS

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Synthesis of Heterocycles
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0591
Electrochemical Reduction of Arenes

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0592
CuH-Mediated Regiodivergent Synthesis of Chiral Alkylated Indoles

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0593
Enantioselective Synthesis of Pentacyclic Spirooxindoles

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0594
Synthesis of γ-Arylated Butenolides by Palladium or Copper Catalysis

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0595
A C–H Bond Alkenylation/Aza-Michael Route to Benzoisothiazole 1-Oxides

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0596
Synthesis of Substituted Benzimidazoles by C–H Imination

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0597
Nitrene C–H Bond Insertion Strategy for Synthesis of γ-Lactams

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0598
Photoredox Radical/Polar Crossover Synthesis of Nitrogen Heterocycles

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0599
Synthesis of α- and β-C-Glycosyl Arenes by Direct Iridium-Catalyzed Hydroarylation

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0600
Cobalt-Catalyzed Synthesis of Isoquinolines by Using a Traceless Directing Group

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0601
Intramolecular Radical Cyclization of 2-Azaallyls to Benzofuran Derivatives

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0602
Rhodium(II)-Catalyzed Enantioselective Synthesis of N-Substituted 2-Pyridones

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0603
Hexahydro-1H-cyclopenta[c]pyrazolo[1,2-a]pyrazole-1,5(2H)-diones

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0604
9a,10,12,12a-Tetrahydrobenzo[b]cyclopenta[f]pyrrolo[1,2-d][1,4]diazepinones

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Synthesis of Materials and Unnatural Products
z0605
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0605
Everything’s Greener on the Other Graphene FREE ACCESS

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0606
It Takes a Pretty Copper to Cyclize

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0607
A Modular Approach to Acridinium Photocatalysts

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0608
Ligand-Controlled DArP for n-Type and Ambipolar Mesopolymers

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0609
A New Coupling Partner for Selective Aromatic Functionalization

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0610
Acid-Mediated Synthesis of Substituted Dibenzo- and Dithienoacridines

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0611
Modding Off: Modular Synthesis of 2-Aryl Triazoles Yields Mechanochromic Luminescence

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0612
Singlet Biradical Character in a Polycyclic Zwitterion

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0613
Cook Me and Call Me the Molecular Dice! FREE ACCESS

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0614
Phospholes to Phos-bowls: The First Synthesis of Phosphindolizine Analogues

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0615
Phenol-Yne Polymerization

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0616
[2+1+2+1] Cycloaddition for Fused Unsymmetric Naphthalenes

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Metals in Synthesis
z0617
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0617
Copper-Catalyzed Alkyne–Azide Cycloaddition by Kinetic Resolution FREE ACCESS

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0618
α-Alkylation of β,γ-Unsaturated Carboxylic Acids with Chiral Lithium Amides

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0619
Asymmetric C–H Functionalization Using Chiral Cp^xCo(III) Catalysis FREE ACCESS

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0620
The Directed Metalation Group Dance

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0621
C–H Activation/Diels–Alder/retro-Diels–Alder Cascade

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0622
Photocatalyzed Uranyl C–C Bond Formation

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0623
Nickel-Catalyzed C–O Bond Arylation of Oxalates

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0624
Chemoselective sp³-C–H Activation in Oxidative Coupling to Form Quaternary Centers

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0625
Divergent Additions of N-tert-Butanesulfinylimidates to Acylsilanes

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0626
Chromium-Catalyzed Amidation of Esters

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0627
Synthesis of Azetidines via Strain Release

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0628
‘Frustrated’ Acid/Base Catalyzed Conia-Ene-Type Cyclizations

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0629
Nickel-Catalyzed Nucleophilic Amination of (Hetero)aryl Chlorides

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0630
Photoredox/Diarylborinic Acid Catalyzed Selective C–H Alkylation of Carbohydrates

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0631
Penta-Alkenylated Carboboranes through Cross-Coupling of Monocarboranes with Alkenes

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0632
Isomerization of Alkenes by Dual-Visible-Light-Cobalt Catalysis

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0633
Carbonyl–Carbonyl Metathesis via Photoredox Catalysis

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0634
Enantioselective Benzylic Arylation of C–H Bonds

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0635
Amine Arylation via C–F Bond Activation

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0636
Photocatalytic Alkylation of Heteroarenes

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0637
α-Arylation of Ketones FREE ACCESS

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0638
Copper-Catalyzed Synthesis of Chiral Tertiary Alcohols from 1,3-Dienes and Ketones

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0639
Iridium-Catalyzed C–C Activation Driven by Aromatization

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0640
α,β-Dehydrogenation and Oxidative Cycloalkenylation Catalyzed by Nickel

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0641
Iron-Catalyzed Alkenylation of Organomagnesium Reagents FREE ACCESS

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0642
Enantioselective Bimetallic Synthesis of 6,6-Spiroketals

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0643
Rhodium-Catalyzed Asymmetric Hydroarylation of Chromenes

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0644
Preparation of β-Fluoroalkyl β-Amino Acids

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0645
An Unprecedented C(aryl)–CH₃ Bond Cleavage

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Polymer-Supported Synthesis
z0647
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0647
Cobalt Molybdenum Sulfide-Catalyzed S-Alkylation of Thiols or H₂S with Alcohols FREE ACCESS

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0648
Microporous Supported Platinum Catalyst for Suzuki–Miyaura and Heck Reactions

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0649
Platinum-Catalyzed Reductive Amination of Levulinic Acid To Give Pyrrolidones

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0650
Aziridation of Olefins Catalyzed by Copper Immobilized on Magnetic Nanoparticles

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0651
Cyclization of Diamines with Aldehydes on a Nanoparticulate Cobalt Catalyst

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0652
Nanoparticulate-Nickel-Catalyzed Reductive Amination of Carbonyl Compounds

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0653
Silicone-Coated Palladium or Platinum Hydrogenation Catalysts

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0654
Hydrosilylation of Alkenes Catalyzed by Nickel Carboxylate Metal–Organic Frameworks

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0655
Metal–Organic Framework Catalyst for Knoevenagel Condensations

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0656
Metal–Organic Framework Catalyst for Nozaki–Hiyama Allenylations

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0657
Oxidation of Benzylic Alcohols on Nitrogen and Phosphorus Co-Doped Graphene

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0658
Hydroxylation of Oxime Ethers with Binaphthyl-Stabilized Palladium Nanoparticles

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0659
Palladium-Catalyzed Aminocarbonylation of Iodobenzenes

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0660
Synthesis of Benzo[a]pyrano[2,3-c]phenazines on Sulfonated Graphene Oxide

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Organo- and Biocatalysis
z0661
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0661
Valorization of a Saturated Fatty Acid to Enantioenriched (S)-δ-Decalactone FREE ACCESS

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0662
Organocatalytic Asymmetric Hydroamination of Allenes and Dienes

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0663
Biosynthesis of Streptoseomycin Involves a [6+4] Cycloaddition

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0664
Amination of Sugars and Sugar-Derived Tetrahydrofurans with Transaminases

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0665
Organocatalytic Synthesis of Unsymmetrical 1,2,4,5-Tetrazines

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0666
Halogen Bond Catalyzed Strain-Release Glycosylation

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0667
Biocatalytic Synthesis of d-Tryptophans from Indoles

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0668
Enantioselective Radical Addition to Vinylpyridines by Photoredox Catalysis

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0669
The Shi Epoxidation FREE ACCESS

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Chemistry in Medicine and Biology
z0671
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0671
LYTACs for the Degradation of Secreted and Membrane Proteins FREE ACCESS

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0672
Design and Synthesis of a Selective CDK7 Covalent Inhibitor

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0673
Discovery of New Chemotypes by Deep Screening of an Ultra-large Virtual Library

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0674
Prebiotic Link between RNA and DNA

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0675
Late-Stage Negishi Coupling of Peptides

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0676
A Highly Selective and Potent Small-Molecule Inhibitor of Factor B

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0677
A Far-Red Emitting Ir^III-Complex–Coumarin Dyad for Photodynamic Therapy

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0678
Dual Inhibitors of Anaplastic Lymphoma Kinase and Bromodomain‑4

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0679
Clickable FPP/GGPP Analogues Enable Analysis of Prenylome

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0680
Modification of Phosphinopeptidic Scaffolds by Giese-Type Alkylation

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0681
Development of Fluorescent Ca²⁺ Sensors FREE ACCESS

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Peptide Chemistry
z0683
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0683
Amide N–H Arylation of Pyroglutamate–Histidine Promoted by Nickel(II) Acetate

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0684
Oligomerization of Amino Thioacids by Simple Oxidation

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0685
Palladium-Catalyzed Site-Selective γ-C(sp³)–H Silylation of Peptides FREE ACCESS

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0686
Ruthenium-Catalyzed Dynamic Kinetic Resolution–Asymmetric Hydrogenation

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0687
One-Pot Reaction of Amino Acid Esters with Isocyanates and α-Bromo Ketones

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0688
Palladium-Catalyzed Insertion of Carbenoids into N,O-Aminals

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0689
Synthesis of the C-Terminal Macrocycle of Asperipin-2a

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0690
Peptide Ligation Mediated by a Removable Acyl Transfer Auxiliary

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0691
Thiourea/Boronic Acid Catalyzed Asymmetric Aza-Michael Reaction

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0692
Silver(I)-Promoted Macrocyclization of Linear Peptides

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Flow Chemistry
z0693
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0693
Light-Induced Beckmann Rearrangement in Continuous Flow

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0694
Continuous-Flow Friedel–Crafts Acylation by Zirconium–β-Zeolite Catalysis

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0695
Aldol Condensation Catalyzed by an Immobilized Base in Continuous Flow

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0696
An Immobilized Palladium Catalyst for Cross-Couplings in Continuous Flow

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0697
Gas/Liquid-Phase Microflow Trifluoromethylation with Fluoroform

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Erratum
0698
Xie, J; Sekine, K; Witzel, S; Krämer, P; Rudolph, M; Rominger, F; Hashmi, A S. K: Photochemical Gold-Catalyzed Arylations

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